暂无反应条件数据

1.1: oxalyl dichloride / N,N-dimethyl-formamide / dichloromethane / 1.5 h / Reflux 2.1: triethylamine; magnesium chloride / acetonitrile / 2 h / Cooling with ice-salt bath 2.2: 20 °C / Cooling with ice-salt bath 2.3: 1.5 h / Cooling with ice 3.1: trifluoromethylsulfonic anhydride; triethylamine; triphenyl-phosphine oxide / 1,2-dichloro-ethane / 2 h / 85 °C / Inert atmosphere View Scheme

1.1: triethylamine; magnesium chloride / acetonitrile / 2 h / Cooling with ice-salt bath 1.2: 20 °C / Cooling with ice-salt bath 1.3: 1.5 h / Cooling with ice 2.1: trifluoromethylsulfonic anhydride; triethylamine; triphenyl-phosphine oxide / 1,2-dichloro-ethane / 2 h / 85 °C / Inert atmosphere View Scheme