1,3-二苯基-1,3-二甲基二硅烷合成路线 （共 18 条）
反应条件
indium tribromide; oxygen in tetrahydrofuran
T=20°C; 4 h;
参考文献
Sridhar, Madabhushi; Ramanaiah, Beeram China; Narsaiah, Chinthala; Kumara Swamy, Mudam; Mahesh, Bellam; Kumar Reddy, Mallu Kishore
Tetrahedron Letters, 2009 , vol. 50, # 51 p. 7166 - 7168
反应条件
1: ortho-iodochlorobenzene With isopropylmagnesium chloride lithium chloride complex in tetrahydrofuran; ethylene glycol dimethyl ether
T=-20°C; Inert atmosphere;
2: methyl phenyl chlorosilane With N,N,N',N,-tetramethylethylenediamine in tetrahydrofuran; ethylene glycol dimethyl ether
T=-20 - 20°C; Inert atmosphere;
3: With water; ammonium chloride in tetrahydrofuran; ethylene glycol dimethyl ether
Inert atmosphere;
参考文献
Murakami, Kei; Yorimitsu, Hideki; Oshima, Koichiro
Journal of Organic Chemistry, 2009 , vol. 74, # 3 p. 1415 - 1417
反应条件
bis(cyclopentadienyl)titanium dichloride; n-butyllithium in tetrahydrofuran; hexane
0.5 h; Heating;
参考文献
Bedard, Thomas C.; Corey, Joyce Y.
Journal of Organometallic Chemistry, 1992 , vol. 428, # 3 p. 315 - 333
反应条件
Mg-anode; stainless steel cathode in tetrahydrofuran
144 h; Electrolysis;
参考文献
Grogger, Christa; Loidl, Bernhard; Stueger, Harald; Kammel, Thomas; Pachaly, Bernd
Journal of Organometallic Chemistry, 2006 , vol. 691, # 1-2 p. 105 - 110
反应条件
bis(cyclopentadienyl)titanium dichloride; n-butyllithium in tetrahydrofuran; hexane
1 h; Heating;
参考文献
Bedard, Thomas C.; Corey, Joyce Y.
Journal of Organometallic Chemistry, 1992 , vol. 428, # 3 p. 315 - 333
反应条件
bis(cyclopentadienyl)titanium dichloride; n-butyllithium in tetrahydrofuran; hexane
1.66667 h; Heating; Further byproducts given;
参考文献
Bedard, Thomas C.; Corey, Joyce Y.
Journal of Organometallic Chemistry, 1992 , vol. 428, # 3 p. 315 - 333
反应条件
norborn-2-ene; bis(cyclopentadienyl)titanium dichloride; n-butyllithium in tetrahydrofuran; hexane
1.66667 h; Heating; Further byproducts given;
参考文献
Bedard, Thomas C.; Corey, Joyce Y.
Journal of Organometallic Chemistry, 1992 , vol. 428, # 3 p. 315 - 333
反应条件
norborn-2-ene; bis(cyclopentadienyl)titanium dichloride; n-butyllithium in tetrahydrofuran; hexane
1.66667 h; Heating; Further byproducts given;
参考文献
Bedard, Thomas C.; Corey, Joyce Y.
Journal of Organometallic Chemistry, 1992 , vol. 428, # 3 p. 315 - 333
反应条件
norborn-2-ene; bis(cyclopentadienyl)titanium dichloride; n-butyllithium in tetrahydrofuran; hexane
1.66667 h; Heating; Further byproducts given;
参考文献
Bedard, Thomas C.; Corey, Joyce Y.
Journal of Organometallic Chemistry, 1992 , vol. 428, # 3 p. 315 - 333
参考文献
Harvey et al.
Journal of the American Chemical Society, 1957 , vol. 79, p. 1437
