4-溴吡啶-2,6-二羧酰胺合成路线 (共 3 条)
反应条件
potassium hydroxide; bromine Hofmann rearrangement; 4 h; Heating;
参考文献
Gray, Mark; Goodman, Allan J.; Carroll, Joseph B.; Bardon, Kevin; Markey, Michael; Cooke, Graeme; Rotello, Vincent M.
Organic Letters, 2004 , vol. 6, # 3 p. 385 - 388
反应条件
ammonia in methanol
3 h; Heating;
参考文献
Gray, Mark; Goodman, Allan J.; Carroll, Joseph B.; Bardon, Kevin; Markey, Michael; Cooke, Graeme; Rotello, Vincent M.
Organic Letters, 2004 , vol. 6, # 3 p. 385 - 388
反应条件
1.1: phosphorus pentabromide / 3 h / 90 °C
1.2: 70 percent / CHCl3
2.1: ammonia / methanol / 3 h / Heating
View Scheme
参考文献
Gray, Mark; Goodman, Allan J.; Carroll, Joseph B.; Bardon, Kevin; Markey, Michael; Cooke, Graeme; Rotello, Vincent M.
Organic Letters, 2004 , vol. 6, # 3 p. 385 - 388