反应条件
1: 75 percent / thionyl chloride; pyridine / acetonitrile / 8 h / 25 °C 2: 98.5 percent / Et3N / tetrahydrofuran; acetonitrile / 21 h / 25 °C 3: NaH; dipotassium hydrogenphosphate / dimethylformamide / 20 h / -30 °C 4: 70.3 percent / aq. NaOH / various solvent(s) / 96 h / 20 °C 5: 71.4 percent / NH4HCO2 / Pd(OH)2-C / H2O; methanol / 13 h / Heating View Scheme
参考文献
Takatsuki, Ken-Ichi; Ohgushi, Sumito; Kohmoto, Shigeo; Kishikawa, Keiki; Yamamoto, Makoto
Nucleosides, Nucleotides and Nucleic Acids, 2006 , vol. 25, # 7 p. 719 - 734
