2-氯-5-氰基-3-甲基吡啶合成路线 （共 5 条）
反应条件
in N,N-dimethyl-formamide T=160°C; 6.5 h;
参考文献
Kagabu, Shinzo
Synthetic Communications, 2006 , vol. 36, # 9 p. 1235 - 1245
反应条件
diisobutylaluminium hydride in toluene 4 h; cooling; Title compound not separated from byproducts;
参考文献
Synthetic Communications, , vol. 36, # 9 p. 1235 - 1245
反应条件
1: diisobutyl aluminum hydride / toluene / 4 h / cooling 2: 89 percent / thionyl chloride / CHCl3 / 1 h / Heating View Scheme
参考文献
Kagabu, Shinzo
Synthetic Communications, 2006 , vol. 36, # 9 p. 1235 - 1245
反应条件
1: With diisobutylaluminium hydride in toluene
4 h; cooling;
2: With sodium tetrahydroborate in methanol; water
cooling;
参考文献
Kagabu, Shinzo
Synthetic Communications, 2006 , vol. 36, # 9 p. 1235 - 1245
反应条件
diisobutylaluminium hydride in toluene
4 h; cooling; Title compound not separated from byproducts;
参考文献
Kagabu, Shinzo
Synthetic Communications, 2006 , vol. 36, # 9 p. 1235 - 1245
