1,3-二甲基-5-异戊基-2,4,6(1H,3H,5H)-嘧啶三酮合成路线 （共 3 条）
参考文献
Cope et al.
Journal of the American Chemical Society, 1941 , vol. 63, p. 356
反应条件
1: dicyclohexyl-carbodiimide; 4-(N,N-dimethlyamino)pyridine / dichloromethane / 18.08 h / 0 - 20 °C
2: acetic acid; sodium cyanoborohydride / 2 h / 20 °C
View Scheme
参考文献
Szostak, Michal; Sautier, Brice; Spain, Malcolm; Behlendorf, Maike; Procter, David J.
Angewandte Chemie - International Edition, 2013 , vol. 52, # 48 p. 12559 - 12563
Angew. Chem., 2013 , vol. 125, # 48 p. 12791 - 12795,5
反应条件
1: dicyclohexyl-carbodiimide; 4-(N,N-dimethlyamino)pyridine / dichloromethane / 18.08 h / 0 - 20 °C
2: acetic acid; sodium cyanoborohydride / 2 h / 20 °C
View Scheme
参考文献
Szostak, Michal; Sautier, Brice; Spain, Malcolm; Behlendorf, Maike; Procter, David J.
Angewandte Chemie - International Edition, 2013 , vol. 52, # 48 p. 12559 - 12563
Angew. Chem., 2013 , vol. 125, # 48 p. 12791 - 12795,5
