双(亚乙基二硫醇)四硫代富瓦烯合成路线 （共 99 条）
反应条件
acetic acid; triphenylphosphine in N,N-dimethyl-formamide T=65 - 70°C; 1.5 h;
参考文献
Neiland, O. Ya.; Balodis, K. A.; Khodorkovskii, V. Yu.; Tilika, V. Zh.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1991 , vol. 27, # 9 p. 1034
Khimiya Geterotsiklicheskikh Soedinenii, 1991 , # 9 p. 1278 - 1279
反应条件
phosphorous acid trimethyl ester T=80°C; P=6000480 Torr; 24 h;
参考文献
Yamashita, Yoshiro; Tomura, Masaaki; Tanaka, Shoji
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1990 , # 12 p. 3358 - 3359
反应条件
phosphorous acid trimethyl ester 3 h; Heating;
参考文献
Larsen, Jan; Lenoir, Christine
Synthesis, 1989 , # 2 p. 134
反应条件
acetic acid; triphenylphosphine in N,N-dimethyl-formamide T=20°C; 48 h;
参考文献
Neiland, O. Ya.; Tilika, V. Zh.; Edzhinya, A. S.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1992 , vol. 28, # 8 p. 945 - 950
Khimiya Geterotsiklicheskikh Soedinenii, 1992 , # 8 p. 1122 - 1128
反应条件
triethyl phosphite T=80°C;
参考文献
Misaki, Yohji; Fujiwara, Hideki; Yamabe, Tokio
Journal of Organic Chemistry, 1996 , vol. 61, # 11 p. 3650 - 3656
反应条件
lithium diisopropyl amide in tetrahydrofuran; hexane 1.) -78 deg C, 4 h, 2.) -78 deg C to r.t., overnight;
参考文献
Meline, Ronald L.; Elsenbaumer, Ronald L.
Journal of the Chemical Society - Perkin Transactions 1, 1997 , # 24 p. 3575 - 3576
反应条件
lithium diisopropyl amide in tetrahydrofuran; hexane 1.) -78 deg C, 4 h, 2.) -78 deg C to r.t., overnight;
参考文献
Meline, Ronald L.; Elsenbaumer, Ronald L.
Journal of the Chemical Society - Perkin Transactions 1, 1997 , # 24 p. 3575 - 3576
反应条件
phosphorous acid trimethyl ester T=65°C; 5 h; Title compound not separated from byproducts;
参考文献
Mori, Takehiko; Inokuchi, Hiroo; Kini, Aravinda M.; Williams, Jack M.
Chemistry Letters, 1990 , # 8 p. 1279 - 1282
反应条件
2,4,6,8,10-pentathiabicyclolt;5.3.0gt;dec-1(7)ene-9-thione; triethyl phosphite T=110°C; 2 h;
参考文献
Ikegawa, Shunjiro; Miyawaki, Kenji; Nogami, Takashi; Shirota, Yasuhiko
Bulletin of the Chemical Society of Japan, 1993 , vol. 66, # 9 p. 2770 - 2772
反应条件
4-oxa-2,6,8,10-tetrathiabicyclolt;5.3.0gt;dec-1(7)ene-9-one; triethyl phosphite T=110°C; 2 h;
参考文献
Nakano, Hideyuki; Yamada, Kazuyori; Nogami, Takashi; Shirota, Yasuhiko; Miyamoto, Akihito; Kobayashi, Hayao
Chemistry Letters, 1990 , # 11 p. 2129 - 2132
