双(亚乙基二硫醇)四硫代富瓦烯合成路线 （共 99 条）
反应条件
phosphorous acid trimethyl ester in benzene 6 h; Heating;
参考文献
Journal of the Chemical Society, Chemical Communications, , # 8 p. 821 - 822
反应条件
phosphorous acid trimethyl ester in benzene 18 h; Heating; Yields of byproduct given;
参考文献
Takahashi, Kazuko; Tomitani, Kensuke
Journal of the Chemical Society, Chemical Communications, 1995 , # 8 p. 821 - 822
反应条件
1: sodium tert-butyl sulfide / dimethylformamide / 0.25 h 2: 0.25 h View Scheme
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 21, # 7 p. 1442
Zhurnal Organicheskoi Khimii, , vol. 21, # 7 p. 1582 - 1583
反应条件
1: Hg(OAc)2 / acetic acid 2: P(OEt)3 View Scheme
参考文献
Russian Journal of Organic Chemistry, , vol. 42, # 12 p. 1873 - 1876
反应条件
1: 95 percent / iPr2NEt / CH2Cl2 / 20 °C 2: 97 percent / Hg(OAc)2; AcOH / CHCl3 / 3 h / 20 °C 3: P(OEt)3 / 3 h / 110 °C View Scheme
参考文献
Journal of the Chemical Society. Perkin Transactions 1, , # 4 p. 407 - 414
反应条件
1: 97 percent / Hg(OAc)2; AcOH / CHCl3 / 3 h / 20 °C 2: P(OEt)3 / 3 h / 110 °C View Scheme
参考文献
Journal of the Chemical Society. Perkin Transactions 1, , # 4 p. 407 - 414
反应条件
1: 89 percent / mercury(II) acetate, AcOH / CHCl3 / 1 h / Ambient temperature 2: 28 percent / Et3P / 5 h / 70 °C View Scheme
参考文献
Journal of the Chemical Society - Perkin Transactions 1, , # 21 p. 3173 - 3177
反应条件
1: 48 percent / mercury acetate / acetic acid 2: triethylphosphite / 1 h / Heating View Scheme
参考文献
Russian Journal of Organic Chemistry, , vol. 31, # 11 p. 1533 - 1537
Zhurnal Organicheskoi Khimii, , vol. 31, # 11 p. 1705 - 1710
反应条件
1: 79 percent / mercury acetate / acetic acid; CHCl3 / 2 h / Heating 2: triethyl phosphite / 1 h / 110 °C View Scheme
参考文献
Chemistry of Heterocyclic Compounds (New York, NY, United States), , vol. 29, # 6 p. 652 - 658
Khimiya Geterotsiklicheskikh Soedinenii, , # 6 p. 761 - 768
反应条件
1: 83 percent / SOCl2 / CH2Cl2 / 1) 0.5 h, 0 deg C, 2) 1 h, reflux 2: 34 percent / (EtO)3P / 4 h / 100 °C View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , # 13 p. 1403 - 1410
