5-溴-2-氯苯甲酰胺环丙酯合成路线 (共 2 条)
反应条件
1: 5-bromo-2-chloro-benzoic acid With oxalyl dichloride; N,N-dimethyl-formamide in toluene T=0°C; 3 h; 2: anhydrous cyclopropylamine With N-ethyl-N,N-diisopropylamine in dichloromethane T=0 - 20°C; 17 h;
参考文献
US2009/62342 A1, ;
Page/Page column 8 ;
反应条件
N-ethyl-N,N-diisopropylamine in dichloromethane T=0 - 20°C; 19 h;
参考文献
WO2007/9250 A1, ;
Page/Page column 36 ;
WO 2007/009250 A1