9-{5-O-[(4-甲基苯基)磺酰基]呋喃戊糖基}-9H-嘌呤-6-胺合成路线 (共 5 条)
参考文献
Blackburn; Langston
Tetrahedron Letters, 1991 , vol. 32, # 44 p. 6425 - 6428
反应条件
hydrogen fluoride in acetonitrile 24 h;
参考文献
Davisson, V. Jo; Davis, Darrell R.; Dixit, Vyas M.; Poulter, C. Dale
Journal of Organic Chemistry, 1987 , vol. 52, # 9 p. 1794 - 1801
反应条件
1: 89 percent / 4-(N,N-dimethylamino)pyridine (4-DMAP) / CH2Cl2 / 20 h / 4 °C 2: 73 percent / 2percent aq. HF / acetonitrile / 24 h View Scheme
参考文献
Journal of Organic Chemistry, , vol. 52, # 9 p. 1794 - 1801
反应条件
1: 89 percent / 4-(N,N-dimethylamino)pyridine (4-DMAP) / CH2Cl2 / 20 h / 4 °C 2: 73 percent / 2percent aq. HF / acetonitrile / 24 h View Scheme
参考文献
Journal of Organic Chemistry, , vol. 52, # 9 p. 1794 - 1801
反应条件
lithium azide in N,N-dimethyl-formamide
T=20°C; 48 h; Inert atmosphere;
参考文献
Mattarella, Martin; Berstis, Laura; Baldridge, Kim K.; Siegel, Jay S.
Bioconjugate Chemistry, 2014 , vol. 25, # 1 p. 115 - 128