in water-d2 competition was followed by H-NMR spectroscopy, at 25 ° C;; aq. soln. of known pH evapd. to dryness, residue dissolved in equal amt. of D2O, left until equilibrium was reached (5 weeks);
参考文献
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), , p. 2927 - 2934
in water-d2 competition reaction followed by H-NMR spectroscopy, at 25 ° C at pH 7.5; aq. soln. of known pH evapd. to dryness in vacuo, residue dissolved in equal volume of D2O, and left until equilibrium left (12 weeks);;
参考文献
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), , p. 2927 - 2934
THE UNIVERSITY OF NORTH CAROLINA AT CHAPEL HILL; JAY, Michael; MUMPER, Russell; HUCKLE, James; SADGROVE, Matthew
Patent: WO2014/82046 A1, 2014 ;
Location in patent: Page/Page column 21 ;
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反应条件
in water
mixing, boiling, cooling to room temp. (pptn.); filtration, washing (water), drying (vac.);
参考文献
Napoli; Bucci; Magri
Journal of Thermal Analysis and Calorimetry, 1996 , vol. 46, # 6 p. 1865 - 1873
