1: H2SO4 / heating for few hours 2: 87 percent / CCl4 / 1 h / Heating View Scheme
参考文献
Sheludyakov, V. D.; Sheludyakova, S. V.; Kuznetsova, M. G.; Silkina, N. N.; Mironov, V. F.
J. Gen. Chem. USSR (Engl. Transl.), 1980 , vol. 50, # 4 p. 875 - 881,705 - 711
1: 3,5-dimethyl-1H-pyrazole With tetrabutylammomium bromide; sodium carbonate in water deprotonation; 2: chloroform in water Substitution; 3 h; Heating;
参考文献
Reger, Daniel L.; Grattan, T. Christian; Brown, Kenneth J.; Little, Christine A.; Lamba, Jaydeep J.S.; Rheingold, Arnold L.; Sommer, Roger D.
Journal of Organometallic Chemistry, 2000 , vol. 607, # 1-2 p. 120 - 128
1: 3,5-dimethyl-1H-pyrazole With pyridine in dichloromethane 0.583333 h; cooling; 2: 2-methyl-acryloyl chloride in dichloromethane T=20°C; 3 h; Further stages.;
参考文献
Sibi, Mukund P.; Sausker, Justin B.
Journal of the American Chemical Society, 2002 , vol. 124, # 6 p. 984 - 991
