反应条件
anhydrous methyl chloride; cadmium; copper mixing of Cu and Si; drying (300°C, 5 h, dry nitrogen), rising temp. to 350°C, addn. of MeCl (4 h), removal of MeSiCl3 and Me2SiCl2, Cd addn. at room temp., rising temp. to 300°C, CHCl3 and HCl addn., 40 h; product collection, distn., receiver cooled to -20.degree, dist. of remains in flask,;
参考文献
Han, Joon Soo; Yeon, Seung Ho; Yoo, Bok Ryul; Jung, Il Nam
Organometallics, 1997 , vol. 16, # 1 p. 93 - 95
