1-吗啉基-1-环己烯合成路线 （共 150 条）
反应条件
chloroform; triethylamine
Erhitzen des Reaktionsgemisches mit wss. Salzsaeure; Behandeln des danach erhaltenen Reaktionsprodukts mit wss. Kalilauge bei 100grad.;
参考文献
Huenig; Luecke
Chemische Berichte, 1959 , vol. 92, p. 652,660
反应条件
1: 41 percent / 5 h / 200 °C
2: 87 percent / propanethiol, methyllithium, 10 percent aqu. HCl / hexamethylphosphoric acid triamide; diethyl ether / 0.5 h
View Scheme
参考文献
Gingrich, Henry L.; Roush, David M.; Saun, William A. Van
Journal of Organic Chemistry, 1983 , vol. 48, # 25 p. 4869 - 4873
参考文献
Begley, Michael J.; Mellor, Michael; Pattenden, Gerald
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 8 p. 1905 - 1912
反应条件
methanol; ammonia
T=70°C; 3 h;
参考文献
Tohda; Eiraku; Nakagawa; Usami; Ariga; Kawashima; Tani; Watanabe; Mori
Bulletin of the Chemical Society of Japan, 1990 , vol. 63, # 10 p. 2820 - 2827
反应条件
1.1: toluene / 8 h / 0 °C / Inert atmosphere
1.2: 6.5 h / Inert atmosphere
2.1: zinc(II) chloride / dichloromethane / 9 h / Inert atmosphere; Reflux
View Scheme
参考文献
Kelgtermans, Hans; Dobrzanska, Liliana; Van Meervelt, Luc; Dehaen, Wim
Tetrahedron, 2011 , vol. 67, # 20 p. 3685 - 3689
反应条件
hydrogenchloride; triethylamine
1.) acetonitrile, 14 h, reflux, 2.) 1 h, room temperature; Yield given. Multistep reaction;
参考文献
Scholz, Dieter
Monatshefte fuer Chemie, 1984 , vol. 115, p. 655 - 658
反应条件
boron trifluoride diethyl etherate in dichloromethane
1 h; Ambient temperatureother temperature, other catalyst, other time, other concentration of catalyst; Product distribution;
参考文献
Takazawa, Osamu; Kogami, Kunio; Hayashi, Kazuo
Bulletin of the Chemical Society of Japan, 1984 , vol. 57, # 7 p. 1876 - 1881
反应条件
titanium tetrachloride
1 h; Ambient temperature;
参考文献
Takazawa, Osamu; Kogami, Kunio; Hayashi, Kazuo
Bulletin of the Chemical Society of Japan, 1984 , vol. 57, # 7 p. 1876 - 1881
反应条件
1: With sodium iodide in acetone; acetonitrile
Stork alkylation; 24 h; Heating;
2: With water
Hydrolysis; 2 h; Heating;
参考文献
Stanetty, Peter; Bahardoust, M. Hassan; Mihovilovic, Marko D.; Mereiter, Kurt
Monatshefte fur Chemie, 1999 , vol. 130, # 10 p. 1257 - 1268
反应条件
benzoyl chloride in chloroform
12 h; Heating; Yield given;
参考文献
Klemm, L. H.; Muchiri, Daniel R.; Louris, John N.
Journal of Heterocyclic Chemistry, 1984 , vol. 21, p. 1135 - 1140
