1-吗啉基-1-环己烯合成路线 (共 150 条)
反应条件
methanol in toluene
T=-78°C; 1 h;
参考文献
Momiyama, Norie; Yamamoto, Hisashi
Journal of the American Chemical Society, 2005 , vol. 127, # 4 p. 1080 - 1081
反应条件
N-chloro-succinimide in dichloromethane
T=20°C; 1 h;
参考文献
Vilsmaier, Elmar; Stamm, Thomas; Dauth, Werner; Tetzlaff, Claus; Barth, Stefan
Bulletin des Societes Chimiques Belges, 1992 , vol. 101, # 1 p. 37 - 44
反应条件
sulfur
1.5 h; Heating;
参考文献
Carmack, Marvin; Behforouz, Mohammad; Berchtold, Glenn A.; Berkowitz, Samuel M.; Wiesler, Donald; Barone, Ralph
Journal of Heterocyclic Chemistry, 1989 , vol. 26, p. 1305 - 1318
反应条件
in chloroform
1.) 30 min, reflux, 2.) 1 day, room temperature;
参考文献
Uher, Michal; Foltin, Jozef; Floch, Lubomir
Collection of Czechoslovak Chemical Communications, 1981 , vol. 46, # 11 p. 2696 - 2702
参考文献
Armarego,W.L.F.
Journal of the Chemical Society [Section] C: Organic, 1969 , p. 986 - 990
参考文献
Osske, G.; Szabo, D.; Lorand, T.
Pharmazie, 1988 , vol. 43, # 3 p. 164 - 165
参考文献
Molines,H.; Wakselman,C.
Tetrahedron, 1976 , vol. 32, p. 2099 - 2103
反应条件
(i) dioxane, (ii) aq. NaOH; Multistep reaction;
参考文献
Nakai,T.; Okawara,M.
Bulletin of the Chemical Society of Japan, 1970 , vol. 43, p. 3528 - 3534
反应条件
n-butyllithium; N,N,N',N',tetramethyl-ethylenediamine
1.) room temp., 2.) -20 deg C; Yield given. Multistep reaction;
参考文献
Inagaki, Satoshi; Iwase, Koji; Goto, Naomi
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1984 , p. 2019 - 2022
反应条件
1: NaOMe / (anodic oxidation)
2: aq. HCl / CHCl3
View Scheme
参考文献
Chiba,T. et al.
Journal of Organic Chemistry, 1979 , vol. 44, p. 3519 - 3523