1-吗啉基-1-环己烯合成路线 （共 150 条）
反应条件
(i), (ii) aq. NaOH; Multistep reaction;
参考文献
Bianchetti,G. et al.
Gazzetta Chimica Italiana, 1963 , vol. 93, p. 1726 - 1735
反应条件
hydrogenchloride; triethylamine 1.) CHCl3, room temp., 15 h, 2.) reflux, 5 h; Yield given. Multistep reaction;
参考文献
Murray, Ewan J.; Crowley, Rebecca C.; Truman, Alex; Clarke, Simon R.; Cottam, James A.; Jadhav, Gopal P.; Steele, Victoria R.; O'Shea, Paul; Lindholm, Catharina; Cockayne, Alan; Chhabra, Siri Ram; Chan, Weng C.; Williams, Paul
Journal of Medicinal Chemistry, 2014 , vol. 57, # 6 p. 2813 - 2819
反应条件
triethylamine; palladium diacetate in tetrahydrofuran T=20°C; 2 h;
参考文献
Ishikawa; Uedo; Tani; Saito
Journal of Organic Chemistry, 2001 , vol. 66, # 1 p. 186 - 191
反应条件
4 A molecular sieve; 10percent Pd/C in toluene Heating; Title compound not separated from byproducts.;
参考文献
Organic Letters, , vol. 4, # 15 p. 2557 - 2559
反应条件
sulfur in ethanol T=50 - 55°C; 2 h;
参考文献
Peet, Norton P.; Sunder, Shyam; Barbuch, Robert J.; Vinogradoff, Anna P.
Journal of Heterocyclic Chemistry, 1986 , vol. 23, p. 129 - 134
反应条件
in dichloromethane 1.) -40 deg C, 2.) room temperature, overnight;
参考文献
Tamura, Yasumitsu; Adachi, Masahiro; Kawasaki, Tomomi; Yasuda, Hitoshi; Kita, Yasuyuki
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 1132 - 1135
反应条件
bromine in chloroform T=20°C; 0.2 h;
参考文献
Iranpoor, Nasser; Firouzabadi, Habib; Shaterian, Hamid Reza; Zolfigol
Phosphorus, Sulfur and Silicon and Related Elements, 2002 , vol. 177, # 5 p. 1047 - 1071
参考文献
Reith,B.A. et al.
Journal of Organic Chemistry, 1974 , vol. 39, p. 2728 - 2736
反应条件
20 h; Ambient temperature;
参考文献
Ishihara, Takashi; Seki, Toshio; Ando, Teiichi
Bulletin of the Chemical Society of Japan, 1982 , vol. 55, # 10 p. 3345 - 3346
反应条件
1: 70 percent / xylene / 72 h / 170 °C 2: 68 percent / 10percent palladium on charcoal / decahydronaphthalene / 48 h / Heating View Scheme
参考文献
Cordonnier, Guy; Sliwa, Henri
Journal of Heterocyclic Chemistry, 1987 , vol. 24, p. 111 - 115
