1-吗啉基-1-环己烯合成路线 （共 150 条）
反应条件
in xylene T=170°C; 72 h;
参考文献
Cordonnier, Guy; Sliwa, Henri
Journal of Heterocyclic Chemistry, 1987 , vol. 24, p. 111 - 115
参考文献
Barton,D.H.R. et al.
Journal of the Chemical Society [Section] C: Organic, 1971 , p. 2204 - 2215
反应条件
1: With triethylamine in toluene T=20 - 35°C; 2: With hydrogenchloride; water in toluene 1 h; Reflux;
参考文献
WO2011/13077 A1, ;
Page/Page column 10 ;
反应条件
1: triethylamine / toluene / 20 - 35 °C 2: hydrogenchloride; water / toluene / 1 h / Reflux View Scheme
反应条件
hydrogenchloride 1) CH2Cl2, -20 deg C, 30 min, 2) 40-50 deg C, 30 min; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Adam, Waldemar; Andler, Simone; Heil, Markus; Voerckel, Volker
Journal of Organic Chemistry, 1992 , vol. 57, # 9 p. 2680 - 2682
参考文献
Air Products and Chemicals, Inc.
Patent: US5086178 A1, 1992 ;
参考文献
Air Products and Chemicals, Inc.
Patent: US5086178 A1, 1992 ;
反应条件
accufluorTM in dichloromethane T=-196 - 20°C;
参考文献
Banks, R. Eric; Besheesh, Mohamed K.; Mohialdin-Khaffaf, Suad N.; Sharif, Iqbal
Journal of the Chemical Society - Perkin Transactions 1, 1996 , # 16 p. 2069 - 2076
反应条件
chloroform; triethylamine anschliessendes Erwaermen mit 20prozentig. wss. Salzsaeure und Erhitzen des Reaktionsprodukts mit wss. Kalilauge bis auf 125grad;
参考文献
Huenig et al.
Chemische Berichte, 1958 , vol. 91, p. 129,133
反应条件
sodium tris(acetoxy)borohydride; acetic acid in 1,2-dichloro-ethane 0.166667 h; Ambient temperature;
参考文献
Journal of Organic Chemistry, , vol. 61, # 11 p. 3849 - 3862
