1-吗啉基-1-环己烯合成路线 (共 150 条)
反应条件
4 A molecular sieve; 10percent Pd/C in toluene Heating; Title compound not separated from byproducts.;
参考文献
Organic Letters, , vol. 4, # 15 p. 2557 - 2559
反应条件
di-tert-butylnitroxide radical in N,N-dimethyl-formamide Irradiation;
参考文献
Russell, Glen A.; Wang, Keyang
Journal of Organic Chemistry, 1991 , vol. 56, # 11 p. 3475 - 3479
反应条件
1: Cu(OCOCH3)2 / acetonitrile / 0 - 20 °C 2: aq. HCl View Scheme
参考文献
Kirij; Pasenok; Yagupolskii; Tyrra; Naumann
Journal of Fluorine Chemistry, 2000 , vol. 106, # 2 p. 217 - 221
反应条件
hydrogenchloride; tetramethyl-ammonium fluoride 1) DMF, 70 deg C, 6 h, irradiated, 2) r.t., 3 h; Yield given. Multistep reaction;
参考文献
Chen, Qing-Yun; Li, Zhan-Ting
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1993 , # 6 p. 645 - 648
反应条件
zinc in diethyl ether
参考文献
Senoez, Huelya; Tunoglu, Nazan
Chemical and Pharmaceutical Bulletin, 2003 , vol. 51, # 4 p. 444 - 447
反应条件
chloroform; triethylamine Behandeln des Reaktionsgemisches mit Wasser und Natriumhydrogencarbonat; Erhitzen des Reaktionsprodukts mit wss. Natronlauge.;
参考文献
Huenig; Luecke
Chemische Berichte, 1959 , vol. 92, p. 652,660
反应条件
anschliessendes Behandeln mit Wasser und Natriumhydrogencarbonat und Erhitzen des Reaktionsprodukts mit wss.Natronlauge;
参考文献
Huenig; Luecke
Chemische Berichte, 1959 , vol. 92, p. 652,660
反应条件
in dichloromethane 336 h;
参考文献
Prishchenko, A. A.; Pisarnitskii, D. A.; Livantsov, M. V.; Petrosyan, V. S.
J. Gen. Chem. USSR (Engl. Transl.), 1992 , vol. 62, # 9 p. 2150 - 2152,1772 - 1773
参考文献
Shen, Yan-Hong; Lv, Hui-Chao; Zhao, Liang
Journal of Chemical Research, 2011 , vol. 35, # 6 p. 349 - 351
反应条件
1: With lithium boron tetrafluoride; [Ru(2,2′-bipyridine)3][hexafluorophosphate]2; 2,3,5,6-tetramethyl-p-benzoquinone in aceonitrile T=20°C; 12 h; Inert atmosphereIrradiationMolecular sieve; 2: With water; ammonium chloride in acetonitrile T=20°C; 1 h; Inert atmosphereMolecular sieve;
参考文献
Yasu, Yusuke; Koike, Takashi; Akita, Munetaka
Chemical Communications, 2012 , vol. 48, # 43 p. 5355 - 5357