1-吗啉基-1-环己烯合成路线 （共 150 条）
反应条件
T=130°C; aza-Darzens reaction; 0.166667 h; Microwave irradiationneat (no solvent);
参考文献
Ma, Li-Jian; Inokuchi, Tsutomu
Chemical Communications, 2010 , vol. 46, # 37 p. 7037 - 7039
反应条件
T=130°C; aza-Darzens reaction; 0.166667 h; Microwave irradiationneat (no solvent);
参考文献
Ma, Li-Jian; Inokuchi, Tsutomu
Chemical Communications, 2010 , vol. 46, # 37 p. 7037 - 7039
反应条件
1: dimethylsulfoxide / 10 h / Irradiation 2: 60 percent / aq. HCl / 0.5 h View Scheme
参考文献
Cranwell, Philippa B.; O'Brien, Matthew; Browne, Duncan L.; Koos, Peter; Polyzos, Anastasios; Pena-Lopez, Miguel; Ley, Steven V.
Organic and Biomolecular Chemistry, 2012 , vol. 10, # 30 p. 5774 - 5779
反应条件
sodium amide in tetrahydrofuran
参考文献
Kametani,T. et al.
Journal of the Chemical Society [Section] C: Organic, 1971 , p. 1047 - 1050
反应条件
Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Ghattas, A.-B.A.G.; Jorgensen, K. A.; Lawesson, S.-O.
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, 1982 , vol. 36, # 8 p. 505 - 512
反应条件
1: 1-morpholino-cyclohexene; 2,6-diamino-4-(5-methylfuran-2-yl)-4H-thiopyran-3,5-dicarbonitrile in ethanol 2 h; Heating; 2: 3',4'-dihydroxy-2-chloroacetophenone With potassium hydroxide in ethanol 4 h; Further stages.;
参考文献
Dyachenko
Russian Journal of Organic Chemistry, 2008 , vol. 44, # 3 p. 412 - 420
反应条件
1: With triethylamine in chloroform T=20°C; 14 h; 2: With sulfuric acid 4 h; Heating;
参考文献
Kritzyn; Komissarov
Russian Journal of Bioorganic Chemistry, 2004 , vol. 30, # 5 p. 436 - 440
反应条件
(i), (ii) aq. HCl; Multistep reaction;
参考文献
Molines,H.; Wakselman,C.
Tetrahedron, 1976 , vol. 32, p. 2099 - 2103
反应条件
trichlorophosphate in 1,2-dichloro-ethane cyclocondensation; 4 h; Heating;
参考文献
Boruah, Romesh C.; Ahmed, Shahadat; Sharma, Utpal; Sandhu, Jagir S.
Journal of Organic Chemistry, 2000 , vol. 65, # 3 p. 922 - 925
反应条件
water 1.) dioxane, reflux, 4 h, 2.) dioxane, reflux, 14 h; Yield given. Multistep reaction;
参考文献
Corcoran, Robert C.; Ma, Junning
Journal of the American Chemical Society, 1992 , vol. 114, # 12 p. 4536 - 4542
