1-吗啉基-1-环己烯合成路线 (共 150 条)
反应条件
T=120 - 130°C; 1.5 h;
参考文献
Chemical & Pharmaceutical Bulletin, , vol. 31, # 12 p. 4300 - 4305
反应条件
hydrogenchloride in 1,4-dioxane; chloroform; water; acetic acid; acetone; Petroleum ether
参考文献
Moon,S.; Waxman,B.H.
Journal of Organic Chemistry, 1969 , vol. 34, # 2 p. 288 - 292
反应条件
hydrogenchloride; triethylamine 1.) benzene, reflux, 12 h, 2.) reflux, 4 h; Yield given. Multistep reaction;
参考文献
Darwish; Patel; Miller
Journal of Organic Chemistry, 1993 , vol. 58, # 22 p. 6072 - 6075
反应条件
hydrogen fluoride T=-3 - 10°C; electrolysis;
参考文献
Meinert, H.; Fackler, R.; Mader, J.; Reuter, P.; Roehlke, W.
Journal of Fluorine Chemistry, 1991 , vol. 51, # 1 p. 53 - 73
反应条件
in ethanol 2 h; Heating;
参考文献
Dyachenko
Russian Journal of Organic Chemistry, 2008 , vol. 44, # 3 p. 412 - 420
反应条件
methanol; 9-borabicyclo[3.3.1]nonane dimer 1.) THF, 25 deg C, 3 h; Yield given. Multistep reaction;
参考文献
Journal of the American Chemical Society, , vol. 111, # 1 p. 384 - 386
反应条件
pyridine; p-toluenesulfonyl chloride
1.) DMF, -20 deg C, 30 min, 2.) DMF, -20 deg C, 4 h, RT, 1 d; Yield given. Multistep reaction;
参考文献
Nagayoshi, Tsuyoshi; Saeki, Seitaro; Hamana, Masatomo
Chemical and Pharmaceutical Bulletin, 1981 , vol. 29, # 7 p. 1920 - 1926
反应条件
hydrogenchloride
1.) CHCl3, -15 deg C, 30 min, 2.) ether; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
May, George L.; Pinhey, John T.
Australian Journal of Chemistry, 1982 , vol. 35, # 9 p. 1859 - 1871
反应条件
titanium tetrachloride
1 h; Ambient temperature;
参考文献
Takazawa, Osamu; Kogami, Kunio; Hayashi, Kazuo
Bulletin of the Chemical Society of Japan, 1984 , vol. 57, # 7 p. 1876 - 1881