1-吗啉基-1-环己烯合成路线 （共 150 条）
反应条件
1: NEt3 / CH2Cl2 / 1.) 1.25 h; 2.) 1 h
2: p-TsOH / benzene / Heating
View Scheme
参考文献
Friary, Richard J.; Seidl, Vera; Schwerdt, John H.; Chan, Tze-Ming; Cohen, Marvin P.; et al.
Tetrahedron, 1993 , vol. 49, # 33 p. 7179 - 7192
反应条件
1: in toluene
T=0°C; 8 h; Inert atmosphere;
2: With hydrogenchloride in water
6.5 h; Inert atmosphere;
参考文献
Kelgtermans, Hans; Dobrzanska, Liliana; Van Meervelt, Luc; Dehaen, Wim
Tetrahedron, 2011 , vol. 67, # 20 p. 3685 - 3689
反应条件
in toluene
15 h; Heating;
参考文献
Tsantali, Georgia G.; Dimtsas, John; Tsoleridis, Constantinos A.; Takakis, Ioannis M.
European Journal of Organic Chemistry, 2007 , # 2 p. 258 - 265
反应条件
in tetrahydrofuran
Stirring of mixt. at room temp. for 15 h.; Extg. (ether), washing of ext. (aq. HCL, H2O), drying (Na2SO4), evapn., chromy. (hexane-ethyl acetate), elem. anal.;
参考文献
Itoh, Keiji; Nakanishi, Saburo; Otsuji, Yoshio
Bulletin of the Chemical Society of Japan, 1991 , vol. 64, # 10 p. 2965 - 2977
反应条件
acrylic acid methyl ester
参考文献
Birkofer; Barnikel
Chemische Berichte, 1958 , vol. 91, p. 1996,1998
反应条件
in 1,2,3,4-tetrahydro-naphthalene
14 h; Heating;
参考文献
Rossi; Stradi; Visentin
Tetrahedron, 1990 , vol. 46, # 10 p. 3581 - 3592
反应条件
benzene
Kochen des Reaktionsprodukts mit wss. Methanol;
参考文献
Stork,G. et al.
Journal of the American Chemical Society, 1963 , vol. 85, p. 207 - 222
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Augustine
Journal of Organic Chemistry, 1963 , vol. 28, p. 152,155
参考文献
Augustine; Caputo
Org. Synth. Coll. Vol., 1973 , vol. V, p. 869
反应条件
hydrogen sulfide; sulfur
参考文献
Asinger et al.
Justus Liebigs Annalen der Chemie, 1959 , vol. 627, p. 195,212
参考文献
Asinger et al.
Justus Liebigs Annalen der Chemie, 1959 , vol. 627, p. 195,212
