4-(1-芘基)-1-丁醇合成路线 （共 8 条）
反应条件
borane-THF in tetrahydrofuran T=20°C; Cooling with ice;
参考文献
Bogani, Lapo; Danieli, Chiara; Biavardi, Elisa; Bendiab, Nedjma; Barra, Anne-Laure; Dalcanale, Enrico; Wernsdorfer, Wolfgang; Cornia, Andrea
Angewandte Chemie - International Edition, 2009 , vol. 48, # 4 p. 746 - 750
反应条件
diisobutylaluminium hydride in tetrahydrofuran; hexane T=0 - 20°C; Inert atmosphere;
参考文献
Granzhan, Anton; Teulade-Fichou, Marie-Paule
Tetrahedron, 2009 , vol. 65, # 7 p. 1349 - 1360
反应条件
lithium aluminium tetrahydride in tetrahydrofuran T=20°C; 4 h;
参考文献
Lampkins, Andrew J.; O'Neil, Edward J.; Smith, Bradley D.
Journal of Organic Chemistry, 2008 , vol. 73, # 16 p. 6053 - 6058
反应条件
1: 1.) lithium wire / 1.)-78 deg C, 12 h., 2.) room temp., 12 h. 2: 2.) DDQ / 1.) methanol, -78 deg C, 2.) abs. toluene, reflux, 1h. View Scheme
参考文献
Tetrahedron, , vol. 40, # 10 p. 1701 - 1712
反应条件
in acetonitrile pH=4.8; 0.166667 h;
参考文献
Tetrahedron Letters, , vol. 54, # 39 p. 5341 - 5344
反应条件
1: 4-(pyren-1-yl)butyl alcohol With potassium tert-butylate in toluene T=100°C; 1 h; 2: 1,10-bis-bromodecane in toluene 16 h;
参考文献
Sirs-Lab GmbH
Patent: US7301043 B2, 2007 ;
Location in patent: Page/Page column 9-10 ;
US 7301043 B2
反应条件
carbon tetrabromide; triphenylphosphine in dichloromethane Bromination; substitution;
参考文献
Furuta, Kyoji; Tomokiyo, Keiichiro; Tien Kuo; Ishikawa, Toshihisa; Suzuki, Masaaki
Tetrahedron, 1999 , vol. 55, # 24 p. 7529 - 7540
反应条件
triethylamine in dichloromethane
T=20°C;
参考文献
Priestley, Rodney D.; Mundra, Manish K.; Barnett, Nina J.; Broadbelt, Linda J.; Torkelson, John M.
Australian Journal of Chemistry, 2007 , vol. 60, # 10 p. 765 - 771
