2-乙基己酸-1-甲基乙酯合成路线 (共 5 条)
反应条件
[rhenium(pentacarbonyl)(bromide)] in 1,2-dichloro-ethane
T=80°C; 2 h; Inert atmosphere;
参考文献
Umeda, Rui; Nishimura, Takashi; Kaiba, Kenta; Tanaka, Toshimasa; Takahashi, Yuuki; Nishiyama, Yutaka
Tetrahedron, 2011 , vol. 67, # 38 p. 7217 - 7221
反应条件
4-(N,N-dimethlyamino)pyridine; dicyclohexyl-carbodiimide in dichloromethane
参考文献
Cho, Chang-Yong; Chung, Keun-Woo; Kim, Young-Wun; Kim, Yeong-Joon
Journal of the Korean Chemical Society, 2010 , vol. 54, # 2 p. 234 - 239
反应条件
1: N-methylmorpholine / CH2Cl2 / 2 h / 0 - 5 °C
2: MgBr2 / CH2Cl2 / 96 h / Ambient temperature
View Scheme
参考文献
Kaminska, Janina E.; Kaminski, Zbigniew J.; Gora, Jozef
Synthesis, 1999 , # 4 p. 593 - 596
反应条件
magnesium bromide in dichloromethane
96 h; Ambient temperature; Yield given;
参考文献
Kaminska, Janina E.; Kaminski, Zbigniew J.; Gora, Jozef
Synthesis, 1999 , # 4 p. 593 - 596
反应条件
isopropyl alcohol; zirconium oxide
T=330°C; temperature dependence on the selection and conversion; Product distribution;
参考文献
Takahashi, Kyoko; Shibagaki, Makoto; Kuno, Hideyuki; Matsushita, Hajime
Chemistry Letters, 1989 , p. 1141 - 1144