2,2'-二甲氧基苯偶酰合成路线 （共 24 条）
反应条件
1: ethanol / 24 h / Reflux
2: ethyl mercaptan sodium salt / N,N-dimethyl-formamide / 4 h / Reflux
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参考文献
You, Lei; Cho, Eun Jeong; Leavitt, John; Ma, Li-Chung; Montelione, Gaetano T.; Anslyn, Eric V.; Krug, Robert M.; Ellington, Andrew; Robertus, Jon D.
Bioorganic and Medicinal Chemistry Letters, 2011 , vol. 21, # 10 p. 3007 - 3011
反应条件
1: 50 percent / 85percent hydrazine hydrate / propan-1-ol / 60 h / Heating
2: 17 percent / yellow HgO / xylene / 2 h / Heating
4: 90 percent / PhMe3Si, I2 / 3 h / 110 °C
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参考文献
Larock, Richard C.; Harrison, L. Wayne
Journal of the American Chemical Society, 1984 , vol. 106, # 15 p. 4218 - 4227
反应条件
1: 50 percent / 85percent hydrazine hydrate / propan-1-ol / 60 h / Heating
2: 17 percent / yellow HgO / xylene / 2 h / Heating
View Scheme
参考文献
Weygand; Siebenmark
Chemische Berichte, 1940 , vol. 73, p. 765,769
反应条件
1: AlCl3; nitrobenzene / 55 °C
2: acetic acid; bromine
View Scheme
参考文献
Kuhn; Birkofer; Moeller
Chemische Berichte, 1943 , vol. 76, p. 900,903
