3,3'-二甲氧基安息香合成路线 （共 15 条）
反应条件
iron nitrate (III) 0.00833333 h; microwave irradiation;
参考文献
Zhao; Wang
Journal of Chemical Research - Part S, 2001 , # 2 p. 70 - 71
反应条件
2,2,6,6-tetramethyl-1-piperidinyloxy, free radical; oxygen; copper(II) bis(trifluoromethanesulfonate); (R)-(+)-1,1'-binaphthyl-2,2'-diamine in toluene T=60°C; 4 h; optical yield given as percent eeenantioselective reaction;
参考文献
Alamsetti, Santosh Kumar; Mannam, Sreedevi; Mutupandi, Pandi; Sekar, Govindasamy
Chemistry - A European Journal, 2009 , vol. 15, # 5 p. 1086 - 1090
反应条件
2,2,6,6-tetramethyl-1-piperidinyloxy, free radical; oxygen; copper(II) bis(trifluoromethanesulfonate); (R)-(+)-1,1'-binaphthyl-2,2'-diamine in toluene T=60°C; 6 h; optical yield given as percent eeenantioselective reaction;
参考文献
Alamsetti, Santosh Kumar; Mannam, Sreedevi; Mutupandi, Pandi; Sekar, Govindasamy
Chemistry - A European Journal, 2009 , vol. 15, # 5 p. 1086 - 1090
反应条件
2,2,6,6-tetramethyl-1-piperidinyloxy, free radical; 2,2'-bis(salicylideneamino)-1,1'-binaphthyl; oxygen; anhydrous cobalt diacetate in chloroform T=20°C; 55 h; Resolution of racemate; enantioselective reaction;
参考文献
Alamsetti, Santosh Kumar; Muthupandi, Pandi; Sekar, Govindasamy
Chemistry - A European Journal, 2009 , vol. 15, # 22 p. 5424 - 5427
反应条件
isocyanatocyclohexane in toluene Heating; Yield given;
参考文献
Cameron, James F.; Willson, C. Grant; Frechet, Jean M. J.
Journal of the Chemical Society - Perkin Transactions 1, 1997 , # 16 p. 2429 - 2442
参考文献
US2014/128392 A1, ;
Page/Page column ;
反应条件
in toluene Heating; Yields of byproduct given;
参考文献
Cameron, James F.; Willson, C. Grant; Frechet, Jean M. J.
Journal of the Chemical Society - Perkin Transactions 1, 1997 , # 16 p. 2429 - 2442
反应条件
oxygen; sodium hydride in tetrahydrofuran; mineral oil T=25°C; P=760.051 Torr; 1 h;
参考文献
Kang, Sunhae; Joo, Cheonik; Kim, Sun Min; Han, Hogyu; Yang, Jung Woon
Tetrahedron Letters, 2011 , vol. 52, # 4 p. 502 - 504
反应条件
sodium dithionite; sodium carbonate; racemic thiourea-based bifunctional organocatalyst in diethyl ether; water
T=20°C; 48 h;
参考文献
Procuranti, Barbara; Connon, Stephen J.
Chemical Communications, 2007 , # 14 p. 1421 - 1423
反应条件
1: With naphthalene; lithium in tetrahydrofuran
T=-78 - 20°C; 1 h; Inert atmosphere;
2: With chloro-trimethyl-silane in tetrahydrofuran
T=0 - 20°C; 0.5 h; Inert atmosphere;
参考文献
BIOENERGENIX; McCall, John M.; Romero, Donna L.
Patent: US2014/128392 A1, 2014 ;
Location in patent: Paragraph 0376; 0377 ;
