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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
6706-96-3
合成路线
(共 20 条)
6706-96-3
→
反应条件
66659-59-4
1,2-二(2-甲氧基苯基)乙酮
反应条件
potassium hydroxide; zinc
参考文献
LaForge
Journal of the American Chemical Society, 1933 , vol. 55, p. 3040,3047
6706-96-3
+
15719-64-9
→
反应条件
66659-59-4
1,2-二(2-甲氧基苯基)乙酮
反应条件
T=250 - 300°C; P=70 Torr;
参考文献
Wilson; Read
Journal of the Chemical Society, 1935 , p. 1120,1123
6706-96-3
→
反应条件
6706-92-9
2,2'-二甲氧基苯偶酰
反应条件
iodine; potassium carbonate in tert-butyl alcohol
参考文献
Yildiz, Tuelay; Canta, Nurguel; Yusufoglu, Ayse
Tetrahedron Asymmetry, 2014 , vol. 25, # 4 p. 340 - 347
6706-96-3
→
反应条件
6706-92-9
2,2'-二甲氧基苯偶酰
反应条件
2,2,6,6-tetramethyl-1-piperidinyloxy, free radical; oxygen; copper(II) bis(trifluoromethanesulfonate); (R)-(+)-1,1'-binaphthyl-2,2'-diamine in toluene T=60°C; 144 h; optical yield given as percent ee;
参考文献
Alamsetti, Santosh Kumar; Mannam, Sreedevi; Mutupandi, Pandi; Sekar, Govindasamy
Chemistry - A European Journal, 2009 , vol. 15, # 5 p. 1086 - 1090
6706-96-3
+
1099-45-2
乙氧甲酰基亚甲基三苯基膦
→
反应条件
6706-92-9
2,2'-二甲氧基苯偶酰
+
93098-03-4
+
93098-07-8
反应条件
T=160 - 170°C; 9 h;
参考文献
Ranade, A. C.; Mali, R. S.; Kurnawal, V. M.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1984 , vol. 23, # 6 p. 514 - 517
6706-96-3
→
反应条件
79215-32-0
反应条件
1: 65 percent / conc. hydrochloric acid / dioxane / 5 h / Heating 2: 70 percent / sodium acetate / 3 h / Heating 3: 65 percent / chromic anhydride / acetic acid / 0.5 h / Heating 4: 66 percent / potassium hydroxide / ethanol / 1 h / Heating View Scheme
参考文献
Hishmat; Abd El Rahman; Khalil Kh.; Atta Sh.
Journal of the Indian Chemical Society, 1981 , vol. 58, # 7 p. 697 - 700
6706-96-3
→
反应条件
479-12-9
6H-苯并呋喃并[3,2-c][1]苯并吡喃-6-酮
反应条件
1: 64 percent / CuSO4*5H2O / pyridine; H2O / 2 h / Heating 2: 50 percent / 85percent hydrazine hydrate / propan-1-ol / 60 h / Heating 3: 17 percent / yellow HgO / xylene / 2 h / Heating 5: 90 percent / PhMe3Si, I2 / 3 h / 110 °C View Scheme
参考文献
Larock, Richard C.; Harrison, L. Wayne
Journal of the American Chemical Society, 1984 , vol. 106, # 15 p. 4218 - 4227
6706-96-3
→
反应条件
4986-28-1
反应条件
1: amalgamated tin; aq.-ethanolic HCl 2: pyridine hydrochloride View Scheme
参考文献
LaForge
Journal of the American Chemical Society, 1933 , vol. 55, p. 3040,3047
6706-96-3
→
反应条件
5293-78-7
反应条件
1: 64 percent / CuSO4*5H2O / pyridine; H2O / 2 h / Heating 2: 50 percent / 85percent hydrazine hydrate / propan-1-ol / 60 h / Heating 3: 17 percent / yellow HgO / xylene / 2 h / Heating View Scheme
参考文献
Larock, Richard C.; Harrison, L. Wayne
Journal of the American Chemical Society, 1984 , vol. 106, # 15 p. 4218 - 4227
6706-96-3
→
反应条件
62495-36-7
反应条件
1: 65 percent / conc. hydrochloric acid / dioxane / 5 h / Heating 2: 70 percent / 20percent potassium hydroxide / 1 h / Ambient temperature 3: 55 percent / chromic anhydride / acetic acid / Heating 4: 50 percent / potassium hydroxide / ethanol / Heating View Scheme
参考文献
Hishmat; Abd El Rahman; Khalil Kh.; Atta Sh.
Journal of the Indian Chemical Society, 1981 , vol. 58, # 7 p. 697 - 700
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