8,9,10,11-四氢苯并(a)蒽合成路线 (共 17 条)
反应条件
2,3-dicyano-5,6-dichloro-p-benzoquinone in benzene 0.333333 h; Heating;
参考文献
Mallory, Frank B.; Rudolph, M. Jonathan; Oh, Soon M.
Journal of Organic Chemistry, 1989 , vol. 54, # 19 p. 4619 - 4626
反应条件
2,3-dicyano-5,6-dichloro-p-benzoquinone in water; acetic acid 0.666667 h; Heating;
参考文献
Journal of Organic Chemistry, , vol. 53, # 19 p. 4587 - 4589
反应条件
Ni(Br)2(dppe); cesium fluoride; zinc in acetonitrile
T=80°C; 12 h;
参考文献
Hsieh, Jen-Chieh; Cheng, Chien-Hong
Chemical Communications, 2005 , # 19 p. 2459 - 2461
反应条件
hydrogen; platinum(IV) oxide; iron(II) chloride in hydrogenchloride
P=1034.3 Torr; 4 h; Ambient temperature; Title compound not separated from byproducts;
参考文献
Fu, Peter P.; Lee, Hong M.; Harvey, Ronald G.
Journal of Organic Chemistry, 1980 , vol. 45, # 14 p. 2797 - 2803
反应条件
hydrogen; platinum(IV) oxide in ethyl acetate
P=2585.7 Torr; 44 h; Ambient temperature; Yield given;
参考文献
Fu, Peter P.; Lee, Hong M.; Harvey, Ronald G.
Journal of Organic Chemistry, 1980 , vol. 45, # 14 p. 2797 - 2803
反应条件
sulfuric acid in tert-butyl alcohol; benzene
26 h; Irradiation;
参考文献
Mallory, Frank B.; Rudolph, M. Jonathan; Oh, Soon M.
Journal of Organic Chemistry, 1989 , vol. 54, # 19 p. 4619 - 4626
反应条件
hydrogen; tetra-n-propyl-diborane
T=200°C; P=67505.4 Torr; 4 h; Further byproducts given. Title compound not separated from byproducts;
参考文献
Yalpani, Mohamed; Koester, Roland
Chemische Berichte, 1990 , vol. 123, # 4 p. 719 - 724
反应条件
ethanol; platinum; iron(II) chloride
Hydrogenation.weiteres Reagens: wss. HCl;
参考文献
Fieser; Hershberg
Journal of the American Chemical Society, 1937 , vol. 59, p. 2502,2507
反应条件
hydrogen; copper(l) chloride; zinc(II) chloride
T=400°C;
参考文献
Nakatsuyi,Y. et al.
Bulletin of the Chemical Society of Japan, 1978 , vol. 51, p. 618 - 624
反应条件
in benzene
Irradiationopen beaker;
参考文献
Olsen, Robert J.; Minniear, John C.; Overton, W. Mack; Sherrick, John M.
Journal of Organic Chemistry, 1991 , vol. 56, # 3 p. 989 - 991