8,9,10,11-四氢苯并(a)蒽合成路线 （共 17 条）
反应条件
selenium
T=320 - 340°C; Erhitzen unter vermindertem Druck;
参考文献
Cook; McGinnis; Mitchell
Journal of the Chemical Society, 1944 , p. 286,293
Full Text Show Details
Cook; Hewett
Journal of the Chemical Society, 1934 , p. 365,375
反应条件
boron trifluoride diethyl etherate
1.) Benzene, ether, 0-20 deg C, 2.) benzene, reflux, 45 min; Yield given. Multistep reaction;
参考文献
Srinivasa Rao; Balu, Maliakel P.; Ila, Hiriyakkanavar; Junjappa, Hiriyakkanavar
Tetrahedron, 1991 , vol. 47, # 20-21 p. 3499 - 3510
反应条件
boron trifluoride diethyl etherate
1.) Benzene, ether, 0-20 deg C, 2.) benzene, reflux, 45 min; Yield given. Multistep reaction;
参考文献
Srinivasa Rao; Balu, Maliakel P.; Ila, Hiriyakkanavar; Junjappa, Hiriyakkanavar
Tetrahedron, 1991 , vol. 47, # 20-21 p. 3499 - 3510
参考文献
Fieser; Hershberg
Journal of the American Chemical Society, 1937 , vol. 59, p. 2502,2507
反应条件
2,3-dicyano-5,6-dichloro-p-benzoquinone in water; acetic acid
0.666667 h; Heating;
参考文献
Lee, Hongmee; Harvey, Ronald G.
Journal of Organic Chemistry, 1988 , vol. 53, # 19 p. 4587 - 4589
反应条件
methanol; 2,3-dicyano-5,6-dichloro-p-benzoquinone
参考文献
Fu,P.P. et al.
Journal of Organic Chemistry, 1979 , vol. 44, # 24 p. 4265 - 4271
反应条件
1: DDQ, MeOH
2: TsOH
3: (i) tetrachloro-<1,2>benzoquinone, (ii) TsOH
View Scheme
参考文献
Fu,P.P. et al.
Journal of Organic Chemistry, 1979 , vol. 44, # 24 p. 4265 - 4271
