1-(6-甲基-4-嘧啶)-乙酮合成路线 （共 5 条）
反应条件
tert.-butylhydroperoxide; iron(II) sulfate in water
T=10 - 20°C; 0.25 h;
参考文献
Sakamoto; Sakasai; Yamanaka
Chemical and Pharmaceutical Bulletin, 1980 , vol. 28, # 2 p. 571 - 577
反应条件
1: 65 percent / silver nitrate, , ammonium persulfate, conc. H2SO4 / CH2Cl2; H2O
2: benzene; 2-methyl-propan-2-ol / 2 h / Irradiation
View Scheme
参考文献
Rao, C. Janakiram; Agosta, William C.
Journal of Organic Chemistry, 1994 , vol. 59, # 8 p. 2125 - 2131
反应条件
acetone
1 h; Irradiation;
参考文献
Brumfield,M.A.; Agosta,W.C.
Journal of the American Chemical Society, 1988 , vol. 110, p. 6790
反应条件
in tert-butyl alcohol; benzene
2 h; Irradiation;
参考文献
Rao, C. Janakiram; Agosta, William C.
Journal of Organic Chemistry, 1994 , vol. 59, # 8 p. 2125 - 2131
反应条件
potassium hydroxide; hydrazine hydrate
1.) EtOH, reflux, 2 h 2.) diethyleneglycol, 170 deg C, 2 h; Yield given. Multistep reaction;
参考文献
Sakamoto; Sakasai; Yamanaka
Chemical and Pharmaceutical Bulletin, 1980 , vol. 28, # 2 p. 571 - 577
