反应条件
1: 1.) titanium tetrachloride, zinc dust / 1.) THF, CH2Cl2, 30 min., 2.) THF, CH2Cl2, RT, 2 h. 2: 80 percent / sodium bis(2-methoxyethoxy)aluminium hydride / toluene / 4 h 3: 84 percent / pyridinium chlorochromate / CH2Cl2 / 15 h / Ambient temperature View Scheme
参考文献
Cambie, Richard C.; Clark, George R.; Goeth, Michelle E.; Rickard, Clifton E.F.; Rutledge, Peter S.; et al.
Australian Journal of Chemistry, 1989 , vol. 42, # 4 p. 497 - 510
