反应条件
1: 35 percent / sodium ethoxide / toluene / 1 h / Heating
2: diethyl ether / 1 h / Ambient temperature
3: 1.) sodium dihydrobis(2-methoxyethoxy)aluminate, 2.) 25percent HAc / 1.) THF, -20 deg C, 0.5 h, 2.) room temp., 8 h
View Scheme
参考文献
Novak; Baan; Marosfalvi; Szantay
Chemische Berichte, 1980 , vol. 113, # 9 p. 2939 - 2949