2-羟基-5-甲氧基苯甲醛合成路线 （共 150 条）
反应条件
1: tetrahydrofuran / -78 °C 2: manganese dioxide / tetrahydrofuran / 2 h / Ambient temperature View Scheme
参考文献
Yoshida, Masahito; Fujino, Yuta; Saito, Koya; Doi, Takayuki
Tetrahedron, 2011 , vol. 67, # 51 p. 9993 - 9997
反应条件
potassium carbonate in acetone 3 h; Heating / reflux; Product distribution / selectivity;
参考文献
Shanks, Thomas Elbert; Maleski, Robert Joseph
Patent: US2003/199714 A1, 2003 ;
Location in patent: Page/Page column 4 ;
参考文献
Tiemann; Mueller
Chemische Berichte, 1881 , vol. 14, p. 1986
反应条件
1: K2CO3 / butan-2-one 2: aq. KOH / ethanol View Scheme
参考文献
Chapleo, Christopher B.; Myers, Peter L.; Butler, Richard C. M.; Davis, John A.; Doxey, John C.; et al.
Journal of Medicinal Chemistry, 1984 , vol. 27, # 5 p. 570 - 576
反应条件
potassium carbonate; butanone Erwaermen des Reaktionsprodukts mit aethanol. Kalilauge;
参考文献
Birkinshaw et al.
Biochemical Journal, 1957 , vol. 66, p. 188,191
Full Text Show Details
Tanaka
Journal of the American Chemical Society, 1951 , vol. 73, p. 872
反应条件
1: methanol; NaOH / Verdunsten zur Trockne und lassen des Rueckstandes mit 1.5 Tln. Essigsaeureanhydrid und absol.Aether 4-5 Stdn. stehen 2: water; acetic acid; KMnO4 / man erwaermt die erhaltene Loesung mit Natronlauge View Scheme
参考文献
Tiemann; Mueller
Chemische Berichte, 1881 , vol. 14, p. 1986
反应条件
1: CH2Cl2 / 2 h 2: 74 percent / K2CO3 / dimethylformamide / 1.) 5 min, 2.) overnight 3: 90 percent / 0.5 h / 650 °C / 0.01 Torr View Scheme
参考文献
Birkinshaw et al.
Biochemical Journal, 1957 , vol. 66, p. 188,191
Full Text Show Details
Tanaka
Journal of the American Chemical Society, 1951 , vol. 73, p. 872
反应条件
1: Py 2: (i) HC(OEt)3, H3PO4, (ii) /BRN= 605351/, ZnCl2, AcOEt, (iii) aq. NaOAc, AcOH View Scheme
参考文献
Billman; Tonnis
Journal of pharmaceutical sciences, 1971 , vol. 60, # 8 p. 1188 - 1192
反应条件
piperidine in dichloromethane Molecular sieve;
参考文献
Ramachary, Dhevalapally B.; Sakthidevi, Rajasekar
Organic and Biomolecular Chemistry, 2010 , vol. 8, # 19 p. 4259 - 4265
反应条件
1.1: K2CO3 / butan-2-one 2.1: aq. KOH / ethanol 3.1: thionyl chloride / benzene 3.2: ammonia / tetrahydrofuran View Scheme
参考文献
Friedman; Toyne; Goodby; Hird
Journal of Materials Chemistry, 2001 , vol. 11, # 11 p. 2759 - 2772
