H2 in toluene Copper-complex is hydrogenated under 3 atm of H2 in toluene, the color of the soln. changes quickly from yellow to orange (under exclusion of air).; investigation by (1)H NMR;
参考文献
, vol. 7, # 5 p. 1208 - 1213
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反应条件
in toluene byproducts: pyridine; N2 or Ar atmosphere of vac.; stirring (1 h); filtn., concn. (vac.), cooling (-20°C); elem. anal.;
