乙基4-(4-甲氧基苯甲酰基)苯甲酸酯合成路线 （共 10 条）
反应条件
iron (III) acetylacetonate in tetrahydrofuran T=0°C;
参考文献
Duplais, Christophe; Bures, Filip; Sapountzis, Ioannis; Korn, Tobias J.; Cahiez, Gerard; Knochel, Paul
Angewandte Chemie - International Edition, 2004 , vol. 43, # 22 p. 2968 - 2970
反应条件
1: 4-methoxy-benzoyl chloride With indium; chloro-trimethyl-silane; ethylene dibromide; lithium chloride in 1-methyl-pyrrolidin-2-one T=80°C; 3 h; Inert atmosphere; 2: 4-iodobenzoic acid ethyl ester With tris-(dibenzylideneacetone)dipalladium(0) in 1-methyl-pyrrolidin-2-one T=25°C; 3 h; Inert atmosphere;
参考文献
Lee, Dohyung; Ryu, Taekyu; Park, Youngchul; Lee, Phil Ho
Organic Letters, 2014 , vol. 16, # 4 p. 1144 - 1147
反应条件
hydrogenchloride in ethanol
反应条件
1: SOCl2 2: 95 percent / acetonitrile / 0.5 h / Heating 3: 83 percent / iron(III) acetylacetonate / tetrahydrofuran / 0 °C View Scheme
参考文献
Angewandte Chemie - International Edition, , vol. 43, # 22 p. 2968 - 2970
反应条件
1: 95 percent / acetonitrile / 0.5 h / Heating 2: 83 percent / iron(III) acetylacetonate / tetrahydrofuran / 0 °C View Scheme
参考文献
Angewandte Chemie - International Edition, , vol. 43, # 22 p. 2968 - 2970
反应条件
1.1: iPrMgCl / tetrahydrofuran / -40 °C 1.2: 65 percent / tetrahydrofuran 2.1: 74 percent / PCC; 18-crown-6 / CHCl3 View Scheme
参考文献
Chimia, , vol. 57, # 11 p. 685 - 691
反应条件
1.1: iPrMgCl / tetrahydrofuran / -40 °C 1.2: 65 percent / tetrahydrofuran 2.1: 74 percent / PCC; 18-crown-6 / CHCl3 View Scheme
参考文献
Chimia, , vol. 57, # 11 p. 685 - 691
反应条件
1: (i) DMF, (ii) FeCl3, aq. HCl 2: HCl / Heating View Scheme
参考文献
Journal of Medicinal Chemistry, , vol. 21, # 9 p. 889 - 894
反应条件
hydrogenchloride Heating;
参考文献
Journal of Medicinal Chemistry, , vol. 21, # 9 p. 889 - 894
反应条件
1: H2 / Pd-C / ethanol
2: aq. NaOH / ethanol / Heating
View Scheme
参考文献
Diana; Carabateas; Johnson; Williams; Pancic; Collins
Journal of Medicinal Chemistry, 1978 , vol. 21, # 9 p. 889 - 894
