反应条件
1.1: tetrakis(triphenylphosphine)palladium(0) / 1,2-dimethoxy-ethane / 0.17 h / 20 °C
1.2: 79 percent / aq. NaHCO3 / 1,2-dimethoxy-ethane / 4 h / Heating
2.1: POCl3 / 1 h / 20 °C
2.2: 92 percent / 12 h / 70 °C
3.1: 92 percent / AlCl3; LiAlH4 / diethyl ether / 2 h / 20 °C
4.1: 92 percent / aq. H2O2; acetic acod / CH2Cl2 / 3 h / 30 °C
View Scheme
参考文献
Oyaizu, Kenichi; Iwasaki, Tomokazu; Tsukahara, Yoshiaki; Tsuchida, Eishun
Macromolecules, 2004 , vol. 37, # 4 p. 1257 - 1270
