in neat (no solvent)
all manipulations under Ar; solvochemically tin metal and 5 eqiuvalents of alkyl bromide heated at 95°C for 60 min; excess alkyl bromide removed in vac., chromy., recrystd. from THF/CHCl3;
Reifenberg, G. H.; Considine, W. J.
Journal of Organometallic Chemistry, 1967 , vol. 9, p. 505 - 509
Full Text View citing articles Show Details
M and T Chemicals, Inc.
Patent: GB1123153 , 1968 ;
C. A., 1968 , vol. 69, p. 87185