反应条件
water in N,N,N',N',N'',N''-hexamethylphosphoric triamide
byproducts: (C2H5)2GeH2; react. in evacuated quartz tube, equimolar mixt. of Et3GeLi and Me3SiGeEt2Li stirred for 94 h at 25°C; hydrolysis; extn. with ether; not isolated, detected by GLC and mass spectrometry;
参考文献
Bravo-Zhivotovskii, D. A.; Pigarev, S. D.; Vyazankina, O. A.; Vyazankin, N. S.
Journal of General Chemistry USSR (English Translation), 1987 , vol. 57, p. 2440 - 2442
Zhurnal Obshchei Khimii, 1987 , vol. 57, p. 2735 - 2738