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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
顺式-4-庚烯醛
合成路线
（共 28 条）
5009-31-4
(Z)-1-溴-3-己烯
+
201230-82-2
→
反应条件
6728-31-0
顺式-4-庚烯醛
反应条件
2,2'-azo-bisisobutyronitrile; tri-n-butyl-tin hydride in benzene T=80°C; P=49400 Torr; 3 h;
参考文献
Ryu, Ilhyong; Kusano, Kazuya; Ogawa, Akiya; Kambe, Nobuaki; Sonoda, Noboru
Journal of the American Chemical Society, 1990 , vol. 112, # 3 p. 1295 - 1297
6191-71-5
顺-4-庚烯-1-醇
→
反应条件
6728-31-0
顺式-4-庚烯醛
反应条件
pyridinium chlorochromate in dichloromethane 2 h;
参考文献
Bestmann; Koschatzky; Schaetzke; et al.
1981 , vol. No. 9, p. 1705 - 1720
21891-36-1
→
反应条件
6728-31-0
顺式-4-庚烯醛
反应条件
hydrogen in ethanol
参考文献
Naarden International N.V.
Patent: US4235824 A1, 1980 ;
16400-32-1
1-溴-2-戊炔
→
反应条件
6728-31-0
顺式-4-庚烯醛
反应条件
1: 60 percent / benzene / 12 h / Heating 2: 65 percent / NaCl, H2O / dimethylsulfoxide / 8 h / 160 °C 3: 76 percent / LAH, EtOH / diethyl ether 4: 80 percent / H2, quinoline / Lindlar's catalyst / hexane 5: 58 percent / pyridinium chlorochromate, NaOAc / CH2Cl2 / 4 h View Scheme
参考文献
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, , vol. 24, p. 313 - 314
42397-24-0
→
反应条件
6728-31-0
顺式-4-庚烯醛
反应条件
1: 80 percent / H2, quinoline / Lindlar's catalyst / hexane 2: 58 percent / pyridinium chlorochromate, NaOAc / CH2Cl2 / 4 h View Scheme
参考文献
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, , vol. 24, p. 313 - 314
6261-22-9
2-戊炔-1-醇
→
反应条件
6728-31-0
顺式-4-庚烯醛
反应条件
1: 77 percent / PBr3, pyridine / diethyl ether / Ambient temperature 2: 60 percent / benzene / 12 h / Heating 3: 65 percent / NaCl, H2O / dimethylsulfoxide / 8 h / 160 °C 4: 76 percent / LAH, EtOH / diethyl ether 5: 80 percent / H2, quinoline / Lindlar's catalyst / hexane 6: 58 percent / pyridinium chlorochromate, NaOAc / CH2Cl2 / 4 h View Scheme
参考文献
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, , vol. 24, p. 313 - 314
98442-18-3
→
反应条件
6728-31-0
顺式-4-庚烯醛
反应条件
1: 65 percent / NaCl, H2O / dimethylsulfoxide / 8 h / 160 °C 2: 76 percent / LAH, EtOH / diethyl ether 3: 80 percent / H2, quinoline / Lindlar's catalyst / hexane 4: 58 percent / pyridinium chlorochromate, NaOAc / CH2Cl2 / 4 h View Scheme
参考文献
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, , vol. 24, p. 313 - 314
98442-19-4
→
反应条件
6728-31-0
顺式-4-庚烯醛
反应条件
1: 76 percent / LAH, EtOH / diethyl ether 2: 80 percent / H2, quinoline / Lindlar's catalyst / hexane 3: 58 percent / pyridinium chlorochromate, NaOAc / CH2Cl2 / 4 h View Scheme
参考文献
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, , vol. 24, p. 313 - 314
530086-82-9
→
反应条件
6728-31-0
顺式-4-庚烯醛
反应条件
1: 74 percent / conc. H2SO4 / acetone; H2O / 20 °C 2: 65 percent / NACAA / CH2Cl2; pyridine / 0.33 h / 20 °C View Scheme
参考文献
Tetrahedron, , vol. 59, # 4 p. 567 - 573
39924-27-1
顺式-4-庚酸乙酯
→
反应条件
6728-31-0
顺式-4-庚烯醛
反应条件
1: 82 percent / LiAlH4 / diethyl ether 2: 76 percent / pyridinium chlorochromate / CH2Cl2 / 2 h View Scheme
参考文献
, vol. No. 9, p. 1705 - 1720
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