2,3,4,5-四氢苯并[c]氮杂-1-酮合成路线 (共 23 条)
反应条件
1: 85 percent / 4 h / 225 °C 2: 100 percent / diethyl ether / 1.) 0 deg C, 2.) room temperature 3: 1.) B2H6, 2.) NaOCH3 / 1.) THF, room temperature, 2.) CH3OH, 2.5 h View Scheme
参考文献
Synthetic Communications, , vol. 12, # 5 p. 373 - 380
反应条件
1: 100 percent / diethyl ether / 1.) 0 deg C, 2.) room temperature 2: 1.) B2H6, 2.) NaOCH3 / 1.) THF, room temperature, 2.) CH3OH, 2.5 h View Scheme
参考文献
Synthetic Communications, , vol. 12, # 5 p. 373 - 380
反应条件
palladium diacetate; triphenylphosphine
参考文献
Meyers, A. I.; Hutchings, Richard H.
Tetrahedron, 1993 , vol. 49, # 9 p. 1807 - 1820
反应条件
1: NH4OH 2: NaBH4, HOAc 3: 30 percent / PPh3, Pd(OAc)2 View Scheme
参考文献
Tetrahedron, , vol. 49, # 9 p. 1807 - 1820
反应条件
1: SOCl2 2: NH4OH 3: NaBH4, HOAc 4: 30 percent / PPh3, Pd(OAc)2 View Scheme
参考文献
Tetrahedron, , vol. 49, # 9 p. 1807 - 1820
反应条件
1: NaBH4, HOAc 2: 30 percent / PPh3, Pd(OAc)2 View Scheme
参考文献
Tetrahedron, , vol. 49, # 9 p. 1807 - 1820
反应条件
1: BH3 2: 30 percent / PPh3, Pd(OAc)2 View Scheme
参考文献
Tetrahedron, , vol. 49, # 9 p. 1807 - 1820
反应条件
2: BH3 3: 30 percent / PPh3, Pd(OAc)2 View Scheme
参考文献
Tetrahedron, , vol. 49, # 9 p. 1807 - 1820
反应条件
sodium methylate; diborane 1.) THF, room temperature, 2.) CH3OH, 2.5 h; Yield given. Multistep reaction;
参考文献
Synthetic Communications, , vol. 12, # 5 p. 373 - 380
反应条件
PPa T=120°C; 2.5 h; other time, temperature; Product distribution;
参考文献
Chemistry of Heterocyclic Compounds (New York, NY, United States), , vol. 19, # 5 p. 528 - 533
Khimiya Geterotsiklicheskikh Soedinenii, , vol. 19, # 5 p. 655 - 660