sodium tetrahydroborate in propan-1-ol T=90°C; P=760.051 Torr; 0.25 h; Microwave irradiationInert atmosphereGreen chemistry;

in tetrahydrofuran; dichloromethane under N2; ratio of Mo(CO)6:dppf:TMNO = 1:0.4:0.8; using TMNO as an initiator; stirred at 28°C for 3.5 h; removal solvents in vacuo; residue extracted with CH2Cl2; soln. applied to silica TLC; elution with 20percent CH2Cl2 in hexane; recrystn. from CH2Cl2/hexane; elem. anal.;