5-甲氧基-2-吡啶羧酸1-氧化物合成路线 （共 2 条）
反应条件
phosphorus oxytribromide T=80°C; 3 h;
参考文献
F. HOFFMANN-LA ROCHE AG; BISSANTZ, Caterina; GRETHER, Uwe; HEBEISEN, Paul; KIMBARA, Atsushi; LIU, Qingping; NETTEKOVEN, Matthias; PRUNOTTO, Marco; ROEVER, Stephan; ROGERS-EVANS, Mark; SCHULZ-GASCH, Tanja; ULLMER, Christoph; WANG, Zhiwei; YANG, Wulun
Patent: WO2012/168350 A1, 2012 ;
Location in patent: Page/Page column 138 ;
WO 2012/168350 A1
反应条件
urea hydrogen peroxide addition compound; trifluoroacetic anhydride in dichloromethane
T=0 - 20°C; 1.5 h;
参考文献
Rouchet, Jean-Baptiste; Schneider, Cedric; Spitz, Cedric; Lefevre, Johan; Dupas, George; Fruit, Corinne; Hoarau, Christophe
Chemistry - A European Journal, 2014 , vol. 20, # 13 p. 3610 - 3615
