pyridine; 4-(N,N-dimethlyamino)pyridine in tetrahydrofuran
T=0 - 20°C;
参考文献
Murphy, Amanda R.; Frechet, Jean M. J.; Chang, Paul; Lee, Josephine; Subramanian, Vivek
Journal of the American Chemical Society, 2004 , vol. 126, # 6 p. 1596 - 1597
1: 87 percent / LiAlH4 / tetrahydrofuran / 2 h / 0 °C
2: 69 percent / pyridine; dimethylaminopyridine / tetrahydrofuran / 0 - 20 °C
View Scheme
参考文献
Murphy, Amanda R.; Frechet, Jean M. J.; Chang, Paul; Lee, Josephine; Subramanian, Vivek
Journal of the American Chemical Society, 2004 , vol. 126, # 6 p. 1596 - 1597
Murphy, Amanda R.; Frechet, Jean M. J.; Chang, Paul; Lee, Josephine; Subramanian, Vivek
Journal of the American Chemical Society, 2004 , vol. 126, # 6 p. 1596 - 1597
1: 72 percent / SnCl4 / CH2Cl2 / 3 h / 0 - 20 °C
2: 87 percent / LiAlH4 / tetrahydrofuran / 2 h / 0 °C
3: 69 percent / pyridine; dimethylaminopyridine / tetrahydrofuran / 0 - 20 °C
View Scheme
参考文献
Murphy, Amanda R.; Frechet, Jean M. J.; Chang, Paul; Lee, Josephine; Subramanian, Vivek
Journal of the American Chemical Society, 2004 , vol. 126, # 6 p. 1596 - 1597
