2-羟基-4-甲氧基苯甲醛合成路线 （共 227 条）
参考文献
de Kiewiet; Stephen
Journal of the Chemical Society, 1931 , p. 639
反应条件
2: pyridine, piperidine / 6 h / 105 °C
View Scheme
参考文献
Hofer, Otmar; Szabo, Geza; Greger, Harald
Monatshefte fuer Chemie, 1986 , vol. 117, p. 1219 - 1222
反应条件
1: α-bromoacetophenone With thiamine hydrochloride in ethanol
T=20°C; 0.25 h; Green chemistry;
2: 2-Hydroxy-4-methoxy-benzaldehyde in ethanol
T=20°C; 1.41667 h; Green chemistry;
参考文献
Mishra, Priya; Singh, Sarita; Ankit, Preyas; Fatma, Shahin; Singh, Divya; Singh, Jagdamba
Bulletin of the Korean Chemical Society, 2013 , vol. 34, # 4 p. 1070 - 1076
反应条件
1.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -78 °C / Inert atmosphere
1.2: 1.5 h / -78 - 0 °C / Inert atmosphere
1.3: 0 °C
2.1: manganese(IV) oxide / acetone / 20 °C / Inert atmosphere
3.1: trifluorormethanesulfonic acid / 1,2-dichloro-ethane / 17 h / 0 - 40 °C / Inert atmosphere
View Scheme
参考文献
Yoshida, Masahito; Fujino, Yuta; Saito, Koya; Doi, Takayuki
Tetrahedron, 2011 , vol. 67, # 51 p. 9993 - 9997
反应条件
1: tetrafluoroboric acid diethyl ether complex / dichloromethane / 1 h / 25 - 30 °C / |Inert atmosphere
2: diisobutylaluminium hydride / dichloromethane; hexane / -78 - 20 °C
View Scheme
参考文献
Fowler, Katherine J.; Ellis, Jillian L.; Morrow, Gary W.
Synthetic Communications, 2013 , vol. 43, # 12 p. 1676 - 1682
反应条件
in ethanol
0.25 h; Heating;
参考文献
Syamal, A.; Kale, K. S.
Indian Journal of Chemistry, Section A: Inorganic, Physical, Theoretical & Analytical, 1980 , vol. 19, # 5 p. 488 - 491
反应条件
sodium hydroxide; (benzyl)-tri-(butyl)-ammonium chloride in dichloromethane
Ambient temperature;
参考文献
Rohlmann, Renate; Daniliuc, Constantin-Gabriel; Mancheno, Olga Garcia
Chemical Communications, 2013 , vol. 49, # 99 p. 11665 - 11667
参考文献
Moafi, Leila; Ahadi, Somayeh; Bazgir, Ayoob
Tetrahedron Letters, 2010 , vol. 51, # 48 p. 6270 - 6274
反应条件
in toluene
T=60°C; Wittig reaction;
参考文献
Gagey, Nathalie; Neveu, Pierre; Benbrahim, Chouaha; Goetz, Bernard; Aujard, Isabelle; Baudin, Jean-Bernard; Jullien, Ludovic
Journal of the American Chemical Society, 2007 , vol. 129, # 32 p. 9986 - 9998
反应条件
potassium carbonate in toluene
T=85°C; 36 h;
参考文献
Behrenswerth, Andrea; Volz, Nicole; Toraeng, Jakob; Hinz, Sonja; Braese, Stefan; Mueller, Christa E.
Bioorganic and Medicinal Chemistry, 2009 , vol. 17, # 7 p. 2842 - 2851
