4-溴硼酸重氮苯四氟硼酸盐合成路线 (共 121 条)
反应条件
NOBF4 in dichloromethane; acetonitrile T=-30°C; 1 h;
参考文献
Bahr; Yang; Kosynkin; Bronikowski; Smalley; Tour
Journal of the American Chemical Society, 2001 , vol. 123, # 27 p. 6536 - 6542
反应条件
sodium nitrite in water T=-5 - 0°C; 0.666667 h;
参考文献
Angewandte Chemie - International Edition, , vol. 53, # 3 p. 725 - 728
Angew. Chem., , vol. 126, # 3 p. 743 - 747,5
反应条件
palladium diacetate; SIDip*HCl in 1,4-dioxane T=100°C; P=760 Torr; 5 h;
参考文献
Andrus, Merritt B.; Ma, Yudao; Zang, Yunfu; Song, Chun
Tetrahedron Letters, 2002 , vol. 43, # 50 p. 9137 - 9140
反应条件
in dichloromethane Schiemann reaction; 336 h; Heating;
参考文献
Wassmundt, Frederick W.; Kiesman, William F.
Journal of Organic Chemistry, 1997 , vol. 62, # 24 p. 8304 - 8308
参考文献
Laali, Kenneth K.; Okazaki, Takao; Bunge, Scott D.
Journal of Organic Chemistry, 2007 , vol. 72, # 18 p. 6758 - 6762
反应条件
18-crown-6 ether; 1,2-dichloro-ethane T=50°C; Rate constant;
参考文献
Nakazumi, Hiroyuki; Kitao, Teijiro; Zollinger, Heinrich
Journal of Organic Chemistry, 1987 , vol. 52, # 13 p. 2825 - 2830
反应条件
1 Pd/C in methanol T=50°C; Suzuki-Miyaura reaction; 0.5 h; Inert atmosphere;
参考文献
Bonin, Helene; Delbrayelle, Dominique; Demonchaux, Patrice; Gras, Emmanuel
Chemical Communications, 2010 , vol. 46, # 15 p. 2677 - 2679
反应条件
sodium nitrite in water T=51.1 - 69.6°C; Kinetics;
参考文献
Bagal,L.I. et al.
Zhurnal Organicheskoi Khimii, 1969 , vol. 5, # 10 p. 1820 - 1828,1767 - 1774
反应条件
palladium diacetate; SIDip*HCl in 1,4-dioxane T=100°C; P=760 Torr; 5 h;
参考文献
Andrus, Merritt B.; Ma, Yudao; Zang, Yunfu; Song, Chun
Tetrahedron Letters, 2002 , vol. 43, # 50 p. 9137 - 9140
反应条件
palladium 10 on activated carbon in methanol Suzuki-Miyaura cross-coupling; 1 h; RefluxUnder air;
参考文献
Hanna Jr., James M.; Varnedoe, Lee S.; Angel, Brad D.; McClellan, Joshua L.
Letters in Organic Chemistry, 2010 , vol. 7, # 1 p. 1 - 6