4-溴硼酸重氮苯四氟硼酸盐合成路线 (共 121 条)
反应条件
methanol-d4; N-benzyl-1,4-dihydronicotinamide in methanol 0.166667 h; Ambient temperaturewith O2 : other D/H ratio; Mechanism;
参考文献
Yasui, Shinro; Nakamura, Kaoru; Ohno, Atsuyoshi
Tetrahedron Letters, 1983 , vol. 24, # 32 p. 3331 - 3334
反应条件
T=20°C; Photolysis; Quantum yield;
参考文献
Journal of Organic Chemistry, , vol. 70, # 2 p. 603 - 610
反应条件
sodium hydrogen telluride in N,N-dimethyl-formamide
0.25 h;
参考文献
Chen; Qiu; Zhou
Synthetic Communications, 1991 , vol. 21, # 17 p. 1729 - 1734
反应条件
bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; tetra-(n-butyl)ammonium iodide; diethylamine in acetonitrile
T=20°C; Sonogashira coupling; 2 h; Inert atmosphere;
参考文献
Fabrizi, Giancarlo; Goggiamani, Antonella; Sferrazza, Alessio; Cacchi, Sandro
Angewandte Chemie - International Edition, 2010 , vol. 49, # 24 p. 4067 - 4070
反应条件
aluminium hydroxide-supported palladium nanoparticles in methanol
T=20°C; Suzuki-Miyaura cross-coupling; 4 h; chemoselective reaction;
参考文献
Li, Xing; Yan, Xu-Ying; Chang, Hong-Hong; Wang, Li-Chao; Zhang, Yan; Chen, Wen-Wen; Li, Yan-Wei; Wei, Wen-Long
Organic and Biomolecular Chemistry, 2012 , vol. 10, # 3 p. 495 - 497
反应条件
trimethylsilylazide; 1-n-butyl-3-methylimidazolium hexafluorophosphate
T=20°C;
参考文献
Hubbard, Abigail; Okazaki, Takao; Laali, Kenneth K.
Journal of Organic Chemistry, 2008 , vol. 73, # 1 p. 316 - 319
反应条件
sodium hydroxide; TiCl3
2.) cetone, 20 deg C, 2 h; Yield given. Multistep reaction;
参考文献
Citterio, Attilio; Cominelli, Alberto; Bonavoglia, Francesco
Synthesis, 1986 , # 4 p. 308 - 309
反应条件
sodium acetate; sodium carbonate; bis(dibenzylideneacetone)-palladium(0) in dichloromethane
0.416667 h; Ambient temperature; Yield given. Yields of byproduct given;
参考文献
Kikukawa, K.; Nagira, K.; Wada, F.; Matsuda, T.
Tetrahedron, 1981 , vol. 37, p. 31 - 36
反应条件
palladium diacetate in methanol
T=20°C; Heck reaction; 12 h; Inert atmosphereDarkness; regioselective reaction;
参考文献
Cacchi, Sandro; Fabrizi, Giancarlo; Goggiamani, Antonella; Sferrazza, Alessio
Synlett, 2009 , # 8 p. 1277 - 1280
反应条件
potassium acetate; 18-crown-6 ether
1.5 h; Ambient temperature;
参考文献
Beadle, James R.; Korzeniowsky, Stephen H.; Rosenberg, David E.; Garcia-Slanga, Blanche J.; Gokel, George W.
Journal of Organic Chemistry, 1984 , vol. 49, # 9 p. 1594 - 1603