4-溴硼酸重氮苯四氟硼酸盐合成路线 （共 121 条）
反应条件
palladium diacetate; polymethylhydrosiloxane in diethyl ether; acetonitrile P=7355.08 Torr; 4 h;
参考文献
Kikukawa, Kiyoshi; Totoki, Takatoshi; Wada, Fumio; Matsuda, Tsutomu
Journal of Organometallic Chemistry, 1984 , vol. 270, # 3 p. 283 - 288
反应条件
1: With [Pd2(dibenzylideneacetone)3]*dibenzylideneacetone; sodium acetate in acetonitrile T=30°C; Heck reaction; 0.5 h; 2: With hydrogenchloride in water; acetonitrile T=25°C; 0.5 h;
参考文献
Machado, Angelo H.L.; de Sousa, Marcio A.; Patto, Daniela C.S.; Azevedo, Luiz F.S.; Bombonato, Fernanda I.; Correia, Carlos Roque D.
Tetrahedron Letters, 2009 , vol. 50, # 11 p. 1222 - 1225
反应条件
bis-triphenylphosphine-palladium(II) chloride in acetonitrile T=20°C; Stille reaction; 0.5 h;
参考文献
Hosoya, Takamitsu; Aoyama, Hiroshi; Ikemoto, Takaaki; Kihara, Yasutaka; Hiramatsu, Toshiyuki; Endo, Makoto; Suzuki, Masaaki
Bioorganic and Medicinal Chemistry, 2003 , vol. 11, # 5 p. 663 - 673
反应条件
1: 1-bromocyclohexane With chloro-trimethyl-silane; magnesium; ethylene dibromide; lithium chloride; zinc dibromide in tetrahydrofuran T=0 - 25°C; 4 h; Inert atmosphere; 2: With zinc dibromide in tetrahydrofuran T=25°C; 0.166667 h; Inert atmosphere; 3: Br-BDT With chloro-trimethyl-silane in tetrahydrofuran T=-60 - 125°C; Inert atmosphereMicrowave irradiation; regioselective reaction;
参考文献
Synthesis, , # 1 p. 23 - 29
反应条件
palladium diacetate; SIDip*HCl in 1,4-dioxane T=100°C; P=760 Torr; 5 h;
参考文献
Andrus, Merritt B.; Ma, Yudao; Zang, Yunfu; Song, Chun
Tetrahedron Letters, 2002 , vol. 43, # 50 p. 9137 - 9140
反应条件
1 Pd/C in methanol T=50°C; Suzuki-Miyaura reaction; 0.25 h; Inert atmosphere;
参考文献
Bonin, Helene; Delbrayelle, Dominique; Demonchaux, Patrice; Gras, Emmanuel
Chemical Communications, 2010 , vol. 46, # 15 p. 2677 - 2679
反应条件
palladium diacetate; SIDip*HCl in 1,4-dioxane T=100°C; P=760 Torr; 5 h;
参考文献
Tetrahedron Letters, , vol. 43, # 50 p. 9137 - 9140
反应条件
palladium 10 on activated carbon in methanol Suzuki-Miyaura cross-coupling; RefluxUnder air;
参考文献
Hanna Jr., James M.; Varnedoe, Lee S.; Angel, Brad D.; McClellan, Joshua L.
Letters in Organic Chemistry, 2010 , vol. 7, # 1 p. 1 - 6
反应条件
[14C]-iodoacetic acid Etherification; iodination; hydrodediazoniation; 0.166667 h; Heating;
参考文献
Journal of Organic Chemistry, , vol. 62, # 24 p. 8304 - 8308
反应条件
iodine; potassium iodide in dimethyl sulfoxide T=15°C;
参考文献
Synthetic Communications, , vol. 11, # 8 p. 639 - 642
