4-溴硼酸重氮苯四氟硼酸盐合成路线 （共 121 条）
反应条件
biscyclopentadienyliron(II); [14C]-iodoacetic acid in isopropyl alcohol Iodination; hydrodediazoniation; 0.166667 h; Heating;
参考文献
Journal of Organic Chemistry, , vol. 62, # 24 p. 8304 - 8308
反应条件
[14C]-iodoacetic acid Etherification; iodination; hydrodediazoniation; 0.166667 h; Heating;
参考文献
Journal of Organic Chemistry, , vol. 62, # 24 p. 8304 - 8308
反应条件
SIDip*HCl; palladium diacetate in tetrahydrofuran T=20°C; 1.5 h;
参考文献
Ma, Yudao; Song, Chun; Jiang, Wei; Xue, Guoping; Cannon, John F.; Wang, Xiaomei; Andrus, Merritt B.
Organic Letters, 2003 , vol. 5, # 24 p. 4635 - 4638
反应条件
1: tBuCH2CH2B(H)NiPr2; Br-BDT With biscyclopentadienyliron(II) in acetonitrile T=20°C; 2.5 h; 2: With methanol in acetonitrile T=0 - 20°C; 1 h; 3: 2,3-dimethylbutane-2,3-diol in diethyl ether; acetonitrile T=20°C; 4 h; Reagent/catalyst;
参考文献
UNIVERSITE DE BORDEAUX 1; CENTRE NATIONAL DE LA RECHERCHE SCIENTIFIQUE; PUCHEAULT, Mathieu Jonathan Damien; MARCIASINI, Ludovic Daniel Alain; VAULTIER, Michel
Patent: WO2014/9169 A1, 2014 ;
Location in patent: Page/Page column 64 ;
反应条件
in dimethyl sulfoxide T=25°C; 5.33333 h;
参考文献
Tetrahedron, , vol. 42, # 14 p. 4007 - 4016
反应条件
nickel dichloride; zinc in tetrahydrofuran Reduction;
参考文献
Bandgar; Uppalla
Journal of Chemical Research - Part S, 1999 , # 12 p. 714 - 715
反应条件
palladium diacetate; SIDip*HCl in 1,4-dioxane T=100°C; P=760 Torr; 5 h;
参考文献
Tetrahedron Letters, , vol. 43, # 50 p. 9137 - 9140
反应条件
palladium diacetate in methanol T=25°C; Heck cross-coupling; 12 h;
参考文献
Felpin, Francois-Xavier; Miqueu, Karinne; Sotiropoulos, Jean-Marc; Fouquet, Eric; Ibarguren, Oier; Laudien, Julia
Chemistry - A European Journal, 2010 , vol. 16, # 17 p. 5191 - 5204
反应条件
palladium diacetate; SIDip*HCl in 1,4-dioxane T=100°C; P=760 Torr; 5 h;
参考文献
Tetrahedron Letters, , vol. 43, # 50 p. 9137 - 9140
反应条件
methanol-d4; N-benzyl-1,4-dihydronicotinamide in methanol 0.166667 h; Ambient temperaturewith O2 : other D/H ratio; Mechanism;
参考文献
Yasui, Shinro; Nakamura, Kaoru; Ohno, Atsuyoshi
Tetrahedron Letters, 1983 , vol. 24, # 32 p. 3331 - 3334
