反应条件
1: 63.5 percent / 50 °C
2: 1.) LiCl, 2.) methanesulfonyl chloride / 1.) s-collidine, DMF, 0 deg C, 2.) 0 to 25 deg C, 8 h
3: 1.) Mg / 1.) THF, reflux, 2.) RT, 1.5 h
View Scheme
参考文献
Zimmerman, Howard E.; Bunce, Richard A.
Journal of Organic Chemistry, 1982 , vol. 47, # 18 p. 3377 - 3396
