5-异亚丙基-2-甲基-2-乙烯基四氢呋喃合成路线 (共 7 条)
反应条件
pyridinium chlorochromate in dichloromethane T=28°C; 2 h; celite;
参考文献
Baskaran, S.; Islam, I.; Raghavan, Malini; Chandrasekaran, S.
Chemistry Letters, 1987 , p. 1175 - 1178
反应条件
potassium tert-butylate in tetrahydrofuran; tert-butyl alcohol
T=50 - 60°C; 1 h;
参考文献
Baskaran, Sundarababu; Islam, Imadul; Chandrasekaran, Srinivasan
Journal of Organic Chemistry, 1990 , vol. 55, # 3 p. 891 - 895
反应条件
potassium tert-butylate
Yield given. Multistep reaction;
参考文献
Mori, Ichiro; Takai, Kazuhiko; Oshima, Koichiro; Nozaki, Hitosi
Tetrahedron, 1984 , vol. 40, # 20 p. 4013 - 4018
反应条件
1: 85 percent / hydrogen peroxide / tetrahydrofuran / 1.) 0 -> 25 deg C, 2.) 25 deg C, 24 h
2: RhCl3 / Ambient temperature
View Scheme
参考文献
Konstantinovic, S.; Bugarcic, Z.; Marjanovic, Lj.; Gojkovic, S.; Mihailovic, M. Lj.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1998 , vol. 37, # 11 p. 1169 - 1170
反应条件
Rhodium trichloride
Ambient temperature;
参考文献
Konstantinovic, S.; Bugarcic, Z.; Marjanovic, Lj.; Gojkovic, S.; Mihailovic, M. Lj.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1998 , vol. 37, # 11 p. 1169 - 1170
反应条件
1: 200 °C
2: RhCl3 / Ambient temperature
View Scheme
参考文献
Konstantinovic, S.; Bugarcic, Z.; Marjanovic, Lj.; Gojkovic, S.; Mihailovic, M. Lj.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1998 , vol. 37, # 11 p. 1169 - 1170
反应条件
1: 61 percent / triisobutylaluminium / CH2Cl2; hexane / 1 h / Ambient temperature
2: PCC / CH2Cl2
View Scheme
参考文献
Mori, Ichiro; Takai, Kazuhiko; Oshima, Koichiro; Nozaki, Hitosi
Tetrahedron, 1984 , vol. 40, # 20 p. 4013 - 4018