1-L-亮氨酰-L-脯氨酸单(三氟乙酸盐)合成路线 （共 8 条）
反应条件
manganese(III) sulphate; sulfuric acid in water T=26°C; Kinetics; Further Variations:SolventsTemperaturesReagents;
参考文献
International Journal of Chemical Kinetics, , vol. 34, # 7 p. 438 - 444
反应条件
manganese(III) sulphate; sulfuric acid in water T=26°C; Kinetics; Further Variations:SolventsTemperaturesReagents;
参考文献
International Journal of Chemical Kinetics, , vol. 34, # 7 p. 438 - 444
反应条件
1.1: 1-hydroxybenzotriazole; 1-ethyl-3-(3-dimethylaminopropyl)carbodiimide / dimethylformamide / -15 °C
1.2: 91.7 percent / N-methylmorpholine / dimethylformamide / 20 °C
2.1: 95.9 percent / aq. NaOH / methanol / 2 h / 20 °C
3.1: 100 percent / 0.67 h
View Scheme
参考文献
Kumara; Channe Gowda; Rangappa
International Journal of Chemical Kinetics, 2002 , vol. 34, # 7 p. 438 - 444
反应条件
1: 95.9 percent / aq. NaOH / methanol / 2 h / 20 °C
2: 100 percent / 0.67 h
View Scheme
参考文献
Kumara; Channe Gowda; Rangappa
International Journal of Chemical Kinetics, 2002 , vol. 34, # 7 p. 438 - 444
反应条件
1.1: 1-hydroxybenzotriazole; 1-ethyl-3-(3-dimethylaminopropyl)carbodiimide / dimethylformamide / -15 °C
1.2: 91.7 percent / N-methylmorpholine / dimethylformamide / 20 °C
2.1: 95.9 percent / aq. NaOH / methanol / 2 h / 20 °C
3.1: 100 percent / 0.67 h
View Scheme
参考文献
Kumara; Channe Gowda; Rangappa
International Journal of Chemical Kinetics, 2002 , vol. 34, # 7 p. 438 - 444
反应条件
1: 61 percent / 1N NaOH / dioxane / 1 h / Ambient temperature
2: anisole / hexane
View Scheme
参考文献
Abiko; Onodera; Sekino
Chemical and Pharmaceutical Bulletin, 1981 , vol. 29, # 5 p. 1390 - 1397
反应条件
methoxybenzene in hexane
参考文献
Abiko; Onodera; Sekino
Chemical and Pharmaceutical Bulletin, 1981 , vol. 29, # 5 p. 1390 - 1397
参考文献
Kumara; Channe Gowda; Rangappa
International Journal of Chemical Kinetics, 2002 , vol. 34, # 7 p. 438 - 444
